benzyl (3-chlorobenzoyl)(2-((E)-3-oxo-3-phenylprop-1-en-1-yl)phenyl)carbamate

Base Information

Chemical Name:benzyl (3-chlorobenzoyl)(2-((E)-3-oxo-3-phenylprop-1-en-1-yl)phenyl)carbamate
CAS No.:1393131-05-9
Molecular Formula:C₃₀H₂₂ClNO₄
Molecular Weight:495.962
Hs Code.:

Synonyms:benzyl (3-chlorobenzoyl)(2-((E)-3-oxo-3-phenylprop-1-en-1-yl)phenyl)carbamate

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Chemical Property of benzyl (3-chlorobenzoyl)(2-((E)-3-oxo-3-phenylprop-1-en-1-yl)phenyl)carbamate

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Technology Process of benzyl (3-chlorobenzoyl)(2-((E)-3-oxo-3-phenylprop-1-en-1-yl)phenyl)carbamate

There total 4 articles about benzyl (3-chlorobenzoyl)(2-((E)-3-oxo-3-phenylprop-1-en-1-yl)phenyl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 1393131-54-8
benzyl (2-((E)-3-oxo-3-phenylprop-1-en-1-yl)phenyl)carbamate

: 618-46-2
m-Chlorobenzoyl chloride

: 1393131-05-9
benzyl (3-chlorobenzoyl)(2-((E)-3-oxo-3-phenylprop-1-en-1-yl)phenyl)carbamate

Guidance literature:: With dmap; triethylamine; In tetrahydrofuran; at 60 ℃; for 12h; Inert atmosphere;
DOI:10.1039/c2cc33972b

Reference yield:

: (2-formyl-phenyl)-carbamic acid benzyl ester

: 1393131-05-9
benzyl (3-chlorobenzoyl)(2-((E)-3-oxo-3-phenylprop-1-en-1-yl)phenyl)carbamate

Guidance literature:: Multi-step reaction with 2 steps

1: toluene / 12 h / 80 °C / Inert atmosphere

2: dmap; triethylamine / tetrahydrofuran / 12 h / 60 °C / Inert atmosphere

With dmap; triethylamine; In tetrahydrofuran; toluene;
DOI:10.1039/c2cc33972b

Reference yield:

: 5344-90-1
2-Aminobenzyl alcohol

: 1393131-05-9
benzyl (3-chlorobenzoyl)(2-((E)-3-oxo-3-phenylprop-1-en-1-yl)phenyl)carbamate

Guidance literature:: Multi-step reaction with 4 steps

1: potassium carbonate / tetrahydrofuran / 12 h / 20 °C / Inert atmosphere

2: pyridinium chlorochromate / dichloromethane / 4 h / 20 °C / Inert atmosphere

3: toluene / 12 h / 80 °C / Inert atmosphere

4: dmap; triethylamine / tetrahydrofuran / 12 h / 60 °C / Inert atmosphere

With dmap; potassium carbonate; triethylamine; pyridinium chlorochromate; In tetrahydrofuran; dichloromethane; toluene;
DOI:10.1039/c2cc33972b