2-hydroxy-3-benzyloxy-9,10-dimethoxy-13-n-octylprotoberberine chloride

Base Information

Chemical Name:2-hydroxy-3-benzyloxy-9,10-dimethoxy-13-n-octylprotoberberine chloride
CAS No.:1375475-77-6
Molecular Formula:C₃₄H₄₀NO₄*Cl
Molecular Weight:562.149
Hs Code.:

Synonyms:2-hydroxy-3-benzyloxy-9,10-dimethoxy-13-n-octylprotoberberine chloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-hydroxy-3-benzyloxy-9,10-dimethoxy-13-n-octylprotoberberine chloride

Chemical Property:

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Technology Process of 2-hydroxy-3-benzyloxy-9,10-dimethoxy-13-n-octylprotoberberine chloride

There total 4 articles about 2-hydroxy-3-benzyloxy-9,10-dimethoxy-13-n-octylprotoberberine chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 22.0%

: 1375475-63-0
2,3-dihydroxy-9,10-dimethoxy-13-n-octylprotoberberine chloride

: 100-39-0
benzyl bromide

: 1375475-77-6
2-hydroxy-3-benzyloxy-9,10-dimethoxy-13-n-octylprotoberberine chloride

Guidance literature:: 2,3-dihydroxy-9,10-dimethoxy-13-n-octylprotoberberine chloride; benzyl bromide; With potassium hydroxide; In N,N-dimethyl-formamide; at 70 ℃;

With hydrogenchloride; In water;
DOI:10.1016/j.ejmech.2012.03.012

Reference yield:

: 483-15-8
7,8-dihydroberberine

: 1375475-77-6
2-hydroxy-3-benzyloxy-9,10-dimethoxy-13-n-octylprotoberberine chloride

Guidance literature:: Multi-step reaction with 3 steps

1.1: acetic acid / ethanol / 5 h / 85 - 95 °C

1.2: 0.5 h / 20 °C

2.1: 3,5-dihydroxyphenol; sulfuric acid / 90 - 95 °C

3.1: potassium hydroxide / N,N-dimethyl-formamide / 70 °C

With 3,5-dihydroxyphenol; sulfuric acid; acetic acid; potassium hydroxide; In ethanol; N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2012.03.012

Reference yield:

: 633-65-8
berberine chloride

: 1375475-77-6
2-hydroxy-3-benzyloxy-9,10-dimethoxy-13-n-octylprotoberberine chloride

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium tetrahydroborate; potassium carbonate; sodium hydroxide / methanol / 2 h / 20 °C

2.1: acetic acid / ethanol / 5 h / 85 - 95 °C

2.2: 0.5 h / 20 °C

3.1: 3,5-dihydroxyphenol; sulfuric acid / 90 - 95 °C

4.1: potassium hydroxide / N,N-dimethyl-formamide / 70 °C

With sodium tetrahydroborate; 3,5-dihydroxyphenol; sulfuric acid; potassium carbonate; acetic acid; potassium hydroxide; sodium hydroxide; In methanol; ethanol; N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2012.03.012