(5-methyl-2-oxo-1,3-dioxolen-4-yl)methyl 6β-aminopenicillanate p-toluenesulfonate

Base Information

Chemical Name:(5-methyl-2-oxo-1,3-dioxolen-4-yl)methyl 6β-aminopenicillanate p-toluenesulfonate
CAS No.:80715-31-7
Molecular Formula:C₇H₈O₃S*C₁₃H₁₆N₂O₆S
Molecular Weight:500.551
Hs Code.:

Synonyms:(5-methyl-2-oxo-1,3-dioxolen-4-yl)methyl 6β-aminopenicillanate p-toluenesulfonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (5-methyl-2-oxo-1,3-dioxolen-4-yl)methyl 6β-aminopenicillanate p-toluenesulfonate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

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Technology Process of (5-methyl-2-oxo-1,3-dioxolen-4-yl)methyl 6β-aminopenicillanate p-toluenesulfonate

There total 4 articles about (5-methyl-2-oxo-1,3-dioxolen-4-yl)methyl 6β-aminopenicillanate p-toluenesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 80715-31-7
(5-methyl-2-oxo-1,3-dioxolen-4-yl)methyl 6β-aminopenicillanate p-toluenesulfonate

Guidance literature:

Reference yield:

: 551-16-6
6-Aminopenicillanic Acid

: 80715-31-7
(5-methyl-2-oxo-1,3-dioxolen-4-yl)methyl 6β-aminopenicillanate p-toluenesulfonate

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / CH₂Cl₂; methanol / 2 h / Ambient temperature

2: potassium bicarbonate, sodium iodide / ethyl acetate; dimethylformamide / 15 h / Ambient temperature

3: ethyl acetate / 0.5 h / 5 - 10 °C

With potassium hydrogencarbonate; triethylamine; sodium iodide; In methanol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1248/cpb.32.4316

Reference yield:

: 87106-40-9
triethylammonium 6β-(1-methyl-2-methoxycarbonylvinylamino)penicillanate

: 80715-31-7
(5-methyl-2-oxo-1,3-dioxolen-4-yl)methyl 6β-aminopenicillanate p-toluenesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: potassium bicarbonate, sodium iodide / ethyl acetate; dimethylformamide / 15 h / Ambient temperature

2: ethyl acetate / 0.5 h / 5 - 10 °C

With potassium hydrogencarbonate; sodium iodide; In ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1248/cpb.32.4316