6-bromo-4-ethenyl-1-(4-methoxybenzyl)-4-(trifluoromethyl)-1,4-dihydro-2H-3,1-benzoxazin-2-one

Base Information

Chemical Name:6-bromo-4-ethenyl-1-(4-methoxybenzyl)-4-(trifluoromethyl)-1,4-dihydro-2H-3,1-benzoxazin-2-one
CAS No.:1141877-88-4
Molecular Formula:C₁₉H₁₅BrF₃NO₃
Molecular Weight:442.232
Hs Code.:

Synonyms:6-bromo-4-ethenyl-1-(4-methoxybenzyl)-4-(trifluoromethyl)-1,4-dihydro-2H-3,1-benzoxazin-2-one

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Chemical Property of 6-bromo-4-ethenyl-1-(4-methoxybenzyl)-4-(trifluoromethyl)-1,4-dihydro-2H-3,1-benzoxazin-2-one

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Technology Process of 6-bromo-4-ethenyl-1-(4-methoxybenzyl)-4-(trifluoromethyl)-1,4-dihydro-2H-3,1-benzoxazin-2-one

There total 2 articles about 6-bromo-4-ethenyl-1-(4-methoxybenzyl)-4-(trifluoromethyl)-1,4-dihydro-2H-3,1-benzoxazin-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 32315-10-9
bis(trichloromethyl) carbonate

: 1141877-87-3
1-{5-bromo-2-[(4-methoxybenzyl)amino]phenyl}-2,2,2-trifluoroethanone

: 1826-67-1
vinyl magnesium bromide

: 1141877-88-4
6-bromo-4-ethenyl-1-(4-methoxybenzyl)-4-(trifluoromethyl)-1,4-dihydro-2H-3,1-benzoxazin-2-one

Guidance literature:: 1-{5-bromo-2-[(4-methoxybenzyl)amino]phenyl}-2,2,2-trifluoroethanone; vinyl magnesium bromide; In tetrahydrofuran; at 0 ℃; for 4h;

With water; ammonium chloride; In tetrahydrofuran; at 20 ℃; for 0.5h;

bis(trichloromethyl) carbonate; With triethylamine; In toluene;

Reference yield: 83.0%

: 32315-10-9
bis(trichloromethyl) carbonate

: C₁₈H₁₇BrF₃NO₂

: 1141877-88-4
6-bromo-4-ethenyl-1-(4-methoxybenzyl)-4-(trifluoromethyl)-1,4-dihydro-2H-3,1-benzoxazin-2-one

Guidance literature:: With triethylamine; In toluene; at 0 ℃;
DOI:10.1021/jm900915x

Reference yield: 87.0%

: 1141877-88-4
6-bromo-4-ethenyl-1-(4-methoxybenzyl)-4-(trifluoromethyl)-1,4-dihydro-2H-3,1-benzoxazin-2-one

: 1141877-90-8
6-bromo-4-(hydroxymethyl)-1-(4-methoxybenzyl)-4-(trifluoromethyl)-1,4-dihydro-2H-3,1-benzoxazin-2-one

Guidance literature:: 6-bromo-4-ethenyl-1-(4-methoxybenzyl)-4-(trifluoromethyl)-1,4-dihydro-2H-3,1-benzoxazin-2-one; With ozone; In methanol; dichloromethane; at 0 ℃; for 2h;

With sodium tetrahydroborate; In methanol; dichloromethane; at 0 ℃; for 0.166667h;
DOI:10.1021/jm900915x