Technology Process of C25H40N4O8
There total 6 articles about C25H40N4O8 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine;
In
dichloromethane;
at 0 - 20 ℃;
for 13h;
DOI:10.1016/j.bmc.2011.07.008
- Guidance literature:
-
Multi-step reaction with 3 steps
1: sodium azide / N,N-dimethyl-formamide / 12 h / 65 °C / Inert atmosphere
2: triphenylphosphine / tetrahydrofuran; water / 24 h / 20 °C
3: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / dichloromethane / 13 h / 0 - 20 °C
With
sodium azide; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; triphenylphosphine;
In
tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2011.07.008
- Guidance literature:
-
Multi-step reaction with 2 steps
1: triphenylphosphine / tetrahydrofuran; water / 24 h / 20 °C
2: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / dichloromethane / 13 h / 0 - 20 °C
With
benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; triphenylphosphine;
In
tetrahydrofuran; dichloromethane; water;
DOI:10.1016/j.bmc.2011.07.008
