(3R)-3-(methoxymethoxy)-7-phenylheptanal

Base Information

Chemical Name:(3R)-3-(methoxymethoxy)-7-phenylheptanal
CAS No.:821785-92-6
Molecular Formula:C₁₅H₂₂O₃
Molecular Weight:250.338
Hs Code.:

Synonyms:(3R)-3-(methoxymethoxy)-7-phenylheptanal

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Chemical Property of (3R)-3-(methoxymethoxy)-7-phenylheptanal

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Technology Process of (3R)-3-(methoxymethoxy)-7-phenylheptanal

There total 7 articles about (3R)-3-(methoxymethoxy)-7-phenylheptanal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1599468-05-9
(3R)-1-[(4R)-4-benzyl-2-thioxo-1,3-thiazolidin-3-yl]-3-(methoxymethoxy)-7-phenylheptan-1-one

: 821785-92-6
(3R)-3-(methoxymethoxy)-7-phenylheptanal

Guidance literature:: With diisobutylaluminium hydride; In dichloromethane; toluene; at -78 ℃; for 3h;
DOI:10.1002/hlca.201300139

Reference yield:

: 10521-91-2
5-phenylpentan-1-ol

: 821785-92-6
(3R)-3-(methoxymethoxy)-7-phenylheptanal

Guidance literature:: Multi-step reaction with 5 steps

1: 88 percent / 2-iodobenzoic acid / dimethylsulfoxide; tetrahydrofuran / 4 h / 20 °C

2: 82 percent / titanium S-BINOL complex / 12 h / 0 °C

3: 90 percent / DIPEA / CH₂Cl₂ / 3 h / 0 °C

4: OsO₄; NMO / acetone; H₂O / 4 h / 20 °C

5: NaIO₄ / 2 h / 20 °C

With sodium periodate; osmium(VIII) oxide; N-methyl-2-indolinone; 2-Iodobenzoic acid; N-ethyl-N,N-diisopropylamine; titanium S-BINOL; In tetrahydrofuran; dichloromethane; water; dimethyl sulfoxide; acetone; 2: Maruoka asymmetric allylation;
DOI:10.1016/j.tetlet.2004.10.059

Reference yield:

: 36884-28-3
5-phenyl-1-pentanal

: 821785-92-6
(3R)-3-(methoxymethoxy)-7-phenylheptanal

Guidance literature:: Multi-step reaction with 4 steps

1: 82 percent / titanium S-BINOL complex / 12 h / 0 °C

2: 90 percent / DIPEA / CH₂Cl₂ / 3 h / 0 °C

3: OsO₄; NMO / acetone; H₂O / 4 h / 20 °C

4: NaIO₄ / 2 h / 20 °C

With sodium periodate; osmium(VIII) oxide; N-methyl-2-indolinone; N-ethyl-N,N-diisopropylamine; titanium S-BINOL; In dichloromethane; water; acetone; 1: Maruoka asymmetric allylation;
DOI:10.1016/j.tetlet.2004.10.059