S-[p-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyloxy)phenylacetohydroximoyl]-2,3,4,6-tetra-O-acetyl-1-thio-β-D-glucopyranose

Base Information

Chemical Name:S-[p-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyloxy)phenylacetohydroximoyl]-2,3,4,6-tetra-O-acetyl-1-thio-β-D-glucopyranose
CAS No.:1240042-19-6
Molecular Formula:C₃₆H₄₅NO₂₀S
Molecular Weight:843.814
Hs Code.:

Synonyms:S-[p-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyloxy)phenylacetohydroximoyl]-2,3,4,6-tetra-O-acetyl-1-thio-β-D-glucopyranose

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Chemical Property of S-[p-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyloxy)phenylacetohydroximoyl]-2,3,4,6-tetra-O-acetyl-1-thio-β-D-glucopyranose

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Technology Process of S-[p-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyloxy)phenylacetohydroximoyl]-2,3,4,6-tetra-O-acetyl-1-thio-β-D-glucopyranose

There total 1 articles about S-[p-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyloxy)phenylacetohydroximoyl]-2,3,4,6-tetra-O-acetyl-1-thio-β-D-glucopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 19879-84-6
tetraacetyl thioglucose

: C₂₂H₂₆ClNO₁₁

: 1240042-19-6
S-[p-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyloxy)phenylacetohydroximoyl]-2,3,4,6-tetra-O-acetyl-1-thio-β-D-glucopyranose

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 1h;
DOI:10.1002/ejoc.201000246

Reference yield: 76.0%

: 1240042-19-6
S-[p-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyloxy)phenylacetohydroximoyl]-2,3,4,6-tetra-O-acetyl-1-thio-β-D-glucopyranose

: 1240042-24-3
per-O-acetylated 4'-O-(β-D-galactopyranosyl)glucosinalbin

Guidance literature:: S-[p-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyloxy)phenylacetohydroximoyl]-2,3,4,6-tetra-O-acetyl-1-thio-β-D-glucopyranose; With sulfur trioxide pyridine complex; In N,N-dimethyl-formamide; at 50 ℃; for 18h; Inert atmosphere;

With potassium hydrogencarbonate; In water; N,N-dimethyl-formamide;
DOI:10.1002/ejoc.201000246