1-O-acetyl-2-O-(3-O-acetyl-4,6-di-O-benzoyl-2-desoxy-2-phthalimido-β-D-glucopyranosyl)-3,4-di-O-benzoyl-α-L-rhamnopyranose

Base Information

Chemical Name:1-O-acetyl-2-O-(3-O-acetyl-4,6-di-O-benzoyl-2-desoxy-2-phthalimido-β-D-glucopyranosyl)-3,4-di-O-benzoyl-α-L-rhamnopyranose
CAS No.:96961-38-5
Molecular Formula:C₅₂H₄₅NO₁₇
Molecular Weight:955.926
Hs Code.:

Synonyms:1-O-acetyl-2-O-(3-O-acetyl-4,6-di-O-benzoyl-2-desoxy-2-phthalimido-β-D-glucopyranosyl)-3,4-di-O-benzoyl-α-L-rhamnopyranose

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Chemical Property of 1-O-acetyl-2-O-(3-O-acetyl-4,6-di-O-benzoyl-2-desoxy-2-phthalimido-β-D-glucopyranosyl)-3,4-di-O-benzoyl-α-L-rhamnopyranose

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Technology Process of 1-O-acetyl-2-O-(3-O-acetyl-4,6-di-O-benzoyl-2-desoxy-2-phthalimido-β-D-glucopyranosyl)-3,4-di-O-benzoyl-α-L-rhamnopyranose

There total 14 articles about 1-O-acetyl-2-O-(3-O-acetyl-4,6-di-O-benzoyl-2-desoxy-2-phthalimido-β-D-glucopyranosyl)-3,4-di-O-benzoyl-α-L-rhamnopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 108-24-7
acetic anhydride

: 96961-33-0
methyl-2-O-(3-O-acetyl-4,6-di-O-benzoyl-2-desoxy-2-phthalimido-β-D-glucopyranosyl)-3,4-di-O-benzoyl-α-L-rhamnopyranoside

: 96961-38-5
1-O-acetyl-2-O-(3-O-acetyl-4,6-di-O-benzoyl-2-desoxy-2-phthalimido-β-D-glucopyranosyl)-3,4-di-O-benzoyl-α-L-rhamnopyranose

Guidance literature:: With sulfuric acid; at 0 ℃; for 5h;
DOI:10.1016/S0040-4020(01)96688-8

Reference yield:

: 89756-12-7
methyl-3-O-acetyl-4,6-di-O-benzoyl-2-desoxy-2-phthalimido-β-D-glucopyranoside

: 96961-38-5
1-O-acetyl-2-O-(3-O-acetyl-4,6-di-O-benzoyl-2-desoxy-2-phthalimido-β-D-glucopyranosyl)-3,4-di-O-benzoyl-α-L-rhamnopyranose

Guidance literature:: Multi-step reaction with 4 steps

1: 77 percent / conc. H₂SO₄ / 5 h / 20 °C

2: HBr / acetic acid

3: 80 percent / Hg(CN)2 / acetonitrile

4: conc. H₂SO₄

With sulfuric acid; hydrogen bromide; mercury(II) cyanide; In acetic acid; acetonitrile;

Reference yield:

: 96961-29-4
1,3-di-O-acetyl-4,6-di-O-benzoyl-2-desoxy-2-phthalimido-D-glucopyranose

: 96961-38-5
1-O-acetyl-2-O-(3-O-acetyl-4,6-di-O-benzoyl-2-desoxy-2-phthalimido-β-D-glucopyranosyl)-3,4-di-O-benzoyl-α-L-rhamnopyranose

Guidance literature:: Multi-step reaction with 3 steps

1: HBr / acetic acid

2: 80 percent / Hg(CN)2 / acetonitrile

3: conc. H₂SO₄

With sulfuric acid; hydrogen bromide; mercury(II) cyanide; In acetic acid; acetonitrile;