4,4'-dichlorodiphenylnitrosamine

Base Information

• Chemical Name: 4,4'-dichlorodiphenylnitrosamine
• CAS No.: 59501-34-7
• Molecular Formula: C₁₂H₈Cl₂N₂O
• Molecular Weight: 267.114
• Mol file: 59501-34-7.mol

Synonyms:4,4'-dichlorodiphenylnitrosamine

Chemical Property of 4,4'-dichlorodiphenylnitrosamine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4,4'-dichlorodiphenylnitrosamine

There total 6 articles about 4,4'-dichlorodiphenylnitrosamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

bis(4-chlorophenyl)amine (6962-04-5) → 4,4'-dichlorodiphenylnitrosamine (59501-34-7)

Guidance literature:

With hydrogenchloride; sodium nitrite;

DOI:10.1021/jo01105a002

Reference yield:

bromochlorobenzene (106-39-8) → 4,4'-dichlorodiphenylnitrosamine (59501-34-7)

Guidance literature:

Multi-step reaction with 2 steps

1: K₂CO₃; CuI

2: 1.51 g / aq. HCl; NaNO₂ / ethanol / 0.75 h / cooling

With hydrogenchloride; copper(l) iodide; potassium carbonate; sodium nitrite; In ethanol;

DOI:10.1021/ol048250y

Reference yield:

N-(4-chlorophenyl)acetamide (539-03-7) → 4,4'-dichlorodiphenylnitrosamine (59501-34-7)

Guidance literature:

Multi-step reaction with 2 steps

1: K₂CO₃; CuI

2: 1.51 g / aq. HCl; NaNO₂ / ethanol / 0.75 h / cooling

With hydrogenchloride; copper(l) iodide; potassium carbonate; sodium nitrite; In ethanol;

DOI:10.1021/ol048250y

upstream raw materials:

bis(4-chlorophenyl)amine

1,1-di(4-chlorophenyl)hydrazine

bromochlorobenzene

N-(4-chlorophenyl)acetamide

Downstream raw materials:

formic acid-[N',N'-bis-(4-chloro-phenyl)-hydrazide]

(4-chloro-phenyl)-(2,4-dichloro-phenyl)-amine

Tetrakis-<4-chlor-phenyl>-hydrazin

1,1-di(4-chlorophenyl)hydrazine