[(S)-1-((S)-2-Benzyloxycarbonylamino-propionylamino)-ethyl]-phosphonic acid

Base Information

• Chemical Name: [(S)-1-((S)-2-Benzyloxycarbonylamino-propionylamino)-ethyl]-phosphonic acid
• CAS No.: 60668-66-8
• Molecular Formula: C₁₃H₁₉N₂O₆P
• Molecular Weight: 330.277

Synonyms:[(S)-1-((S)-2-Benzyloxycarbonylamino-propionylamino)-ethyl]-phosphonic acid

Chemical Property of [(S)-1-((S)-2-Benzyloxycarbonylamino-propionylamino)-ethyl]-phosphonic acid

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Technology Process of [(S)-1-((S)-2-Benzyloxycarbonylamino-propionylamino)-ethyl]-phosphonic acid

There total 8 articles about [(S)-1-((S)-2-Benzyloxycarbonylamino-propionylamino)-ethyl]-phosphonic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.0%

(S)-1-aminoethylphosphonic acid (66068-76-6) + (N-benzyloxycarbonyl)-L-alanine N-hydroxysuccinimide ester (3401-36-3) → [(S)-1-((S)-2-Benzyloxycarbonylamino-propionylamino)-ethyl]-phosphonic acid (60668-66-8)

Guidance literature:

With sodium hydrogencarbonate; In ethanol; water;

DOI:10.1021/jm00151a005

Reference yield: 38.0%

1-aminoethanephosphonic acid (6323-97-3) + 2,4,5-trichlorophenyl ester N-(benzyloxycarbonyl)-L-alanine (7536-54-1) → 1-R-1-[(N-benzyloxycarbonyl-L-alanyl)amino]ethanephosphonic acid (60668-26-0) + [(S)-1-((S)-2-Benzyloxycarbonylamino-propionylamino)-ethyl]-phosphonic acid (60668-66-8)

Guidance literature:

With triethylamine; In water; N,N-dimethyl-formamide; at 0 - 25 ℃; for 0.5h;

DOI:10.1021/jm00151a005

Reference yield: 27.0%

1-aminoethanephosphonic acid (6323-97-3) + (N-benzyloxycarbonyl)-L-alanine N-hydroxysuccinimide ester (3401-36-3) → 1-R-1-[(N-benzyloxycarbonyl-L-alanyl)amino]ethanephosphonic acid (60668-26-0) + [(S)-1-((S)-2-Benzyloxycarbonylamino-propionylamino)-ethyl]-phosphonic acid (60668-66-8)

Guidance literature:

With triethylamine; In water; N,N-dimethyl-formamide; at 0 - 25 ℃; for 0.5h;

DOI:10.1021/jm00151a005

upstream raw materials:

N-Carbobenzoxy-L-alanin-kohlensaeureaethylesteranhydrid

Diethyl-N-(benzyloxycarbonyl)-L-alanyl-(2-decarboxy-DL-alanin-2-yl)phosphonat

2-((S)-2-Benzyloxycarbonylamino-propionylamino)-propionic acid

N-Cbz-Ala

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