6-dimethylaminomethyl-nicotinic acid Na salt

Base Information

Chemical Name:6-dimethylaminomethyl-nicotinic acid Na salt
CAS No.:914669-96-8
Molecular Formula:C₉H₁₁N₂O₂*Na
Molecular Weight:202.188
Hs Code.:

Synonyms:6-dimethylaminomethyl-nicotinic acid Na salt

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Chemical Property of 6-dimethylaminomethyl-nicotinic acid Na salt

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Technology Process of 6-dimethylaminomethyl-nicotinic acid Na salt

There total 1 articles about 6-dimethylaminomethyl-nicotinic acid Na salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 56026-36-9
methyl 6-(hydroxymethyl)nicotinate

: 914669-96-8
6-dimethylaminomethyl-nicotinic acid Na salt

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / dmap / dichloromethane / 5 h / -78 °C

2: methanol / 5.5 h / 0 - 20 °C

3: sodium hydroxide; water / methanol / 1.5 h / 90 °C

With sodium hydroxide; water; triethylamine; dmap; In methanol; dichloromethane;

Reference yield:

: 914669-96-8
6-dimethylaminomethyl-nicotinic acid Na salt

: 914669-95-7
4-(6-((dimethylamino)methyl)pyridin-3-yl)-N-(4-(pentyloxy)-3-(trifluoromethyl)phenyl)thiazol-2-amine

Guidance literature:: Multi-step reaction with 3 steps

1.1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 1.5 h / 0 - 20 °C

2.1: triethylamine / tetrahydrofuran; diethyl ether / 0 - 20 °C

2.2: 2 h / 0 °C

3.1: ethanol / 2 h / Heating / reflux

With oxalyl dichloride; triethylamine; N,N-dimethyl-formamide; In tetrahydrofuran; diethyl ether; ethanol; dichloromethane;