dichloure de N-p-toluenesulfonyl dioxa-3,9-aza-6-undecanedioyle-1,11

Base Information

Chemical Name:dichloure de N-p-toluenesulfonyl dioxa-3,9-aza-6-undecanedioyle-1,11
CAS No.:78630-99-6
Molecular Formula:C₁₅H₁₉Cl₂NO₆S
Molecular Weight:412.291
Hs Code.:

Synonyms:dichloure de N-p-toluenesulfonyl dioxa-3,9-aza-6-undecanedioyle-1,11

Suppliers and Price of dichloure de N-p-toluenesulfonyl dioxa-3,9-aza-6-undecanedioyle-1,11

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of dichloure de N-p-toluenesulfonyl dioxa-3,9-aza-6-undecanedioyle-1,11

Chemical Property:

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Technology Process of dichloure de N-p-toluenesulfonyl dioxa-3,9-aza-6-undecanedioyle-1,11

There total 5 articles about dichloure de N-p-toluenesulfonyl dioxa-3,9-aza-6-undecanedioyle-1,11 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 78630-98-5
N-p-toluenesulfonyldioxa-3,9-aza-6-undecanedioique-1,11

: 78630-99-6
dichloure de N-p-toluenesulfonyl dioxa-3,9-aza-6-undecanedioyle-1,11

Guidance literature:: With pyridine; oxalyl dichloride; In benzene; for 3h; Ambient temperature;
DOI:10.1002/hlca.19810640410

Reference yield:

: 7146-67-0
N-tosyldiethanolamine

: 78630-99-6
dichloure de N-p-toluenesulfonyl dioxa-3,9-aza-6-undecanedioyle-1,11

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / NaH / tetrahydrofuran / 24 h / 25 °C

2: ClCOCOCl, pyridine / benzene

With pyridine; oxalyl dichloride; sodium hydride; In tetrahydrofuran; benzene;
DOI:10.1039/c39890000608

Reference yield:

: 98-59-9
p-toluenesulfonyl chloride

: 78630-99-6
dichloure de N-p-toluenesulfonyl dioxa-3,9-aza-6-undecanedioyle-1,11

Guidance literature:: Multi-step reaction with 5 steps

1: 80 percent / K₃CO₃ / H₂O / 1 h / 100 °C

2: 98 percent / HCl / CHCl₃ / 0 °C

3: 232 g / dimethylformamide / 1 h / 0 °C

4: 80 percent / Ba(OH)2 / H₂O / 2 h / Heating

5: 95 percent / (COCl)2, pyridine / benzene / 3 h / Ambient temperature

With pyridine; hydrogenchloride; barium dihydroxide; oxalyl dichloride; potassium carbonate; In chloroform; water; N,N-dimethyl-formamide; benzene;
DOI:10.1002/hlca.19810640410