N-propyl-2-(2-hydroxyethyl)aminobenzoic amide

Base Information

Chemical Name:N-propyl-2-(2-hydroxyethyl)aminobenzoic amide
CAS No.:417715-41-4
Molecular Formula:C₁₂H₁₈N₂O₂
Molecular Weight:222.287
Hs Code.:

Synonyms:N-propyl-2-(2-hydroxyethyl)aminobenzoic amide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-propyl-2-(2-hydroxyethyl)aminobenzoic amide

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Technology Process of N-propyl-2-(2-hydroxyethyl)aminobenzoic amide

There total 3 articles about N-propyl-2-(2-hydroxyethyl)aminobenzoic amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.5%

: 56814-10-9
2-amino-N-propylbenzamide

: 540-51-2
2-bromoethanol

: 417715-41-4
N-propyl-2-(2-hydroxyethyl)aminobenzoic amide

Guidance literature:: With sodium hydrogencarbonate; In acetonitrile; for 8h; Heating;
DOI:10.1002/hc.1107

Reference yield:

: 118-48-9
isatoic anhydride

: 417715-41-4
N-propyl-2-(2-hydroxyethyl)aminobenzoic amide

Guidance literature:: Multi-step reaction with 2 steps

1: 96.5 percent / dioxane / 1.5 h / 60 - 70 °C

2: 75.5 percent / sodium bicarbonate / acetonitrile / 8 h / Heating

With sodium hydrogencarbonate; In 1,4-dioxane; acetonitrile;
DOI:10.1002/hc.1107

Reference yield:

: 118-92-3,159201-01-1,50816-84-7,80206-34-4,104809-47-4
anthranilic acid

: 417715-41-4
N-propyl-2-(2-hydroxyethyl)aminobenzoic amide

Guidance literature:: Multi-step reaction with 3 steps

1: 94.4 percent / acetonitrile; pyridine; CH₂Cl₂ / 2 h / 50 - 55 °C

2: 96.5 percent / dioxane / 1.5 h / 60 - 70 °C

3: 75.5 percent / sodium bicarbonate / acetonitrile / 8 h / Heating

With sodium hydrogencarbonate; In 1,4-dioxane; pyridine; dichloromethane; acetonitrile;
DOI:10.1002/hc.1107