Technology Process of C20H23NO3S
There total 5 articles about C20H23NO3S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
water; silver nitrate;
In
acetone;
at 20 ℃;
for 12h;
DOI:10.1021/ja201204g
- Guidance literature:
-
Multi-step reaction with 4 steps
1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 20 °C
2: potassium carbonate / N,N-dimethyl-formamide / 80 °C
3: 1,1'-bis-(diphenylphosphino)ferrocene; palladium diacetate / toluene / 16 h / 120 °C / Inert atmosphere
4: water; silver nitrate / acetone / 12 h / 20 °C
With
1,1'-bis-(diphenylphosphino)ferrocene; di-isopropyl azodicarboxylate; water; palladium diacetate; potassium carbonate; silver nitrate; triphenylphosphine;
In
tetrahydrofuran; N,N-dimethyl-formamide; acetone; toluene;
1: Mitsunobu reaction;
DOI:10.1021/ja201204g
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 1,1'-bis-(diphenylphosphino)ferrocene; palladium diacetate / toluene / 16 h / 120 °C / Inert atmosphere
2: water; silver nitrate / acetone / 12 h / 20 °C
With
1,1'-bis-(diphenylphosphino)ferrocene; water; palladium diacetate; silver nitrate;
In
acetone; toluene;
DOI:10.1021/ja201204g