2-(4-hydroxy-3-methoxyphenyl)-5-(5,5-dimethyl-1,3-dioxan-2-yl)-7-methoxybenzofuran

Base Information

Chemical Name:2-(4-hydroxy-3-methoxyphenyl)-5-(5,5-dimethyl-1,3-dioxan-2-yl)-7-methoxybenzofuran
CAS No.:473240-76-5
Molecular Formula:C₂₂H₂₄O₆
Molecular Weight:384.429
Hs Code.:

Synonyms:2-(4-hydroxy-3-methoxyphenyl)-5-(5,5-dimethyl-1,3-dioxan-2-yl)-7-methoxybenzofuran

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(4-hydroxy-3-methoxyphenyl)-5-(5,5-dimethyl-1,3-dioxan-2-yl)-7-methoxybenzofuran

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Technology Process of 2-(4-hydroxy-3-methoxyphenyl)-5-(5,5-dimethyl-1,3-dioxan-2-yl)-7-methoxybenzofuran

There total 2 articles about 2-(4-hydroxy-3-methoxyphenyl)-5-(5,5-dimethyl-1,3-dioxan-2-yl)-7-methoxybenzofuran which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 332077-64-2
2-(4-benzyloxy-3-methoxyphenyl)-5-(5,5-dimethyl-1,3-dioxan-2-yl)-7-methoxybenzofuran

: 473240-76-5
2-(4-hydroxy-3-methoxyphenyl)-5-(5,5-dimethyl-1,3-dioxan-2-yl)-7-methoxybenzofuran

Guidance literature:: With hydrogen; 10percent Pd-C; In dichloromethane; at 20 ℃; for 30h; under 3102.97 Torr;
DOI:10.1021/jo0258960

Reference yield:

: 2-(p-benzyloxy-m-methoxyphenyl)-3-chloromercurio-5-(5',5'-dimethyl-1',3'-dioxan-2'-yl)-7-methoxybenzofuran

: 473240-76-5
2-(4-hydroxy-3-methoxyphenyl)-5-(5,5-dimethyl-1,3-dioxan-2-yl)-7-methoxybenzofuran

Guidance literature:: Multi-step reaction with 2 steps

1: 4.07 g / sodium borohydride / tetrahydrofuran / 12.5 h / 20 °C

2: 88 percent / hydrogen / 10percent Pd-C / CH₂Cl₂ / 30 h / 20 °C / 3102.97 Torr

With sodium tetrahydroborate; hydrogen; 10percent Pd-C; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jo0258960