2-(4-benzyloxy-3-methoxyphenyl)-5-(5,5-dimethyl-1,3-dioxan-2-yl)-7-methoxybenzofuran

Base Information

• Chemical Name: 2-(4-benzyloxy-3-methoxyphenyl)-5-(5,5-dimethyl-1,3-dioxan-2-yl)-7-methoxybenzofuran
• CAS No.: 332077-64-2
• Molecular Formula: C₂₉H₃₀O₆
• Molecular Weight: 474.554

Synonyms:2-(4-benzyloxy-3-methoxyphenyl)-5-(5,5-dimethyl-1,3-dioxan-2-yl)-7-methoxybenzofuran

Chemical Property of 2-(4-benzyloxy-3-methoxyphenyl)-5-(5,5-dimethyl-1,3-dioxan-2-yl)-7-methoxybenzofuran

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Technology Process of 2-(4-benzyloxy-3-methoxyphenyl)-5-(5,5-dimethyl-1,3-dioxan-2-yl)-7-methoxybenzofuran

There total 2 articles about 2-(4-benzyloxy-3-methoxyphenyl)-5-(5,5-dimethyl-1,3-dioxan-2-yl)-7-methoxybenzofuran which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-(p-benzyloxy-m-methoxyphenyl)-3-chloromercurio-5-(5',5'-dimethyl-1',3'-dioxan-2'-yl)-7-methoxybenzofuran → 2-(4-benzyloxy-3-methoxyphenyl)-5-(5,5-dimethyl-1,3-dioxan-2-yl)-7-methoxybenzofuran (332077-64-2)

Guidance literature:

With potassium hydroxide; sodium tetrahydroborate; In tetrahydrofuran; water;

DOI:10.1016/S0040-4039(00)02163-8

Reference yield:

methanol (67-56-1) + carbon monoxide (201230-82-2) + 2-(p-benzyloxy-m-methoxyphenyl)-3-chloromercurio-5-(5',5'-dimethyl-1',3'-dioxan-2'-yl)-7-methoxybenzofuran → 2-(4-benzyloxy-3-methoxyphenyl)-5-(5,5-dimethyl-1,3-dioxan-2-yl)-7-methoxybenzofuran (332077-64-2) + 2-(4-benzyloxy-3-methoxy-phenyl)-5-(5,5-dimethyl-[1,3]dioxan-2-yl)-7-methoxy-benzofuran-3-carboxylic acid methyl ester; compound with mercury(II) chloride

Guidance literature:

With magnesium oxide; lithium chloride; palladium dichloride; at -78 ℃; for 5.5h;

DOI:10.1021/jo0258960

Reference yield: 92.0%

2-(4-benzyloxy-3-methoxyphenyl)-5-(5,5-dimethyl-1,3-dioxan-2-yl)-7-methoxybenzofuran (332077-64-2) → 2-(4-benzyloxy-3-methoxyphenyl)-7-methoxybenzo[b]furan-5-carboxaldehyde (332077-65-3)

Guidance literature:

With hydrogenchloride; water; In acetone; at 20 ℃;

DOI:10.1016/S0040-4039(00)02163-8

upstream raw materials:

methanol

carbon monoxide

Downstream raw materials:

2-(4-benzyloxy-3-methoxyphenyl)-7-methoxybenzo[b]furan-5-carboxaldehyde

2-(4-hydroxy-3-methoxyphenyl)-5-(5,5-dimethyl-1,3-dioxan-2-yl)-7-methoxybenzofuran

(E)-2-(4-hydroxy-3-methoxyphenyl)-5-(3-hydroxyprop-1-enyl)-7-methoxybenzofuran

2-(p-hydroxy-m-methoxyphenyl)-7-methoxy-5-(carbethoxy-1-propen-1-yl)benzo[b]furan

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