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C36H39N7O6S2

Base Information
  • Chemical Name:C36H39N7O6S2
  • CAS No.:1333378-30-5
  • Molecular Formula:C36H39N7O6S2
  • Molecular Weight:729.881
  • Hs Code.:
C<sub>36</sub>H<sub>39</sub>N<sub>7</sub>O<sub>6</sub>S<sub>2</sub>

Synonyms:C36H39N7O6S2

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Chemical Property of C36H39N7O6S2
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Technology Process of C36H39N7O6S2

There total 18 articles about C36H39N7O6S2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With sodium azide; In N,N-dimethyl-formamide; at 80 ℃; for 4h;
DOI:10.1002/ejoc.201100242
Guidance literature:
Multi-step reaction with 12 steps
1: acetic acid; zinc / water / 1.83 h / 80 - 85 °C
2: glyoxylic acid ethyl ester; magnesium sulfate / dichloromethane / 0 - 20 °C
3: dmap; triethylamine / toluene / 18 h / 70 °C
4: ammonium cerium (IV) nitrate / water; acetonitrile / 0.25 h / -15 °C
5: dichloromethane / 4 h / 20 °C
6: copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); triethylamine / 1,4-dioxane / 21 h / 100 °C
7: tetrabutyl ammonium fluoride / tetrahydrofuran; water / 0.33 h / 0 °C
8: hydrogen bromide; acetic acid / tetrahydrofuran / 0.5 h / 0 °C
9: tetrakis(triphenylphosphine) palladium(0); sodium ethanolate; caesium carbonate / 1,4-dioxane / 4 h / 100 °C
10: lithium borohydride / tetrahydrofuran / 0 - 20 °C
11: dmap; triethylamine / dichloromethane / 10 h / 20 °C
12: sodium azide / N,N-dimethyl-formamide / 4 h / 80 °C
With dmap; copper(l) iodide; lithium borohydride; tetrakis(triphenylphosphine) palladium(0); sodium azide; glyoxylic acid ethyl ester; ammonium cerium (IV) nitrate; tetrabutyl ammonium fluoride; hydrogen bromide; sodium ethanolate; magnesium sulfate; caesium carbonate; acetic acid; triethylamine; zinc; In tetrahydrofuran; 1,4-dioxane; dichloromethane; water; N,N-dimethyl-formamide; toluene; acetonitrile; 6: Sonogashira coupling / 9: Suzuki-Miyaura cross-coupling reaction;
DOI:10.1002/ejoc.201100242
Guidance literature:
Multi-step reaction with 10 steps
1: dmap; triethylamine / toluene / 18 h / 70 °C
2: ammonium cerium (IV) nitrate / water; acetonitrile / 0.25 h / -15 °C
3: dichloromethane / 4 h / 20 °C
4: copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); triethylamine / 1,4-dioxane / 21 h / 100 °C
5: tetrabutyl ammonium fluoride / tetrahydrofuran; water / 0.33 h / 0 °C
6: hydrogen bromide; acetic acid / tetrahydrofuran / 0.5 h / 0 °C
7: tetrakis(triphenylphosphine) palladium(0); sodium ethanolate; caesium carbonate / 1,4-dioxane / 4 h / 100 °C
8: lithium borohydride / tetrahydrofuran / 0 - 20 °C
9: dmap; triethylamine / dichloromethane / 10 h / 20 °C
10: sodium azide / N,N-dimethyl-formamide / 4 h / 80 °C
With dmap; copper(l) iodide; lithium borohydride; tetrakis(triphenylphosphine) palladium(0); sodium azide; ammonium cerium (IV) nitrate; tetrabutyl ammonium fluoride; hydrogen bromide; sodium ethanolate; caesium carbonate; acetic acid; triethylamine; In tetrahydrofuran; 1,4-dioxane; dichloromethane; water; N,N-dimethyl-formamide; toluene; acetonitrile; 4: Sonogashira coupling / 7: Suzuki-Miyaura cross-coupling reaction;
DOI:10.1002/ejoc.201100242
upstream raw materials:

C20H21BrN2O4

C27H27BrN2O6S

C20H21BrN2O5S

C25H29BrN2O7S

Downstream raw materials:

C31H31N7O4S2

C41H35BrN8O6S2

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