benzyl [2-[(3S)-4-hydroxy-2,6-dimethylheptan-3-ylamino]-2-oxoethyl]carbamate

Base Information

• Chemical Name: benzyl [2-[(3S)-4-hydroxy-2,6-dimethylheptan-3-ylamino]-2-oxoethyl]carbamate
• CAS No.: 1596798-44-5
• Molecular Formula: C₁₉H₃₀N₂O₄
• Molecular Weight: 350.458

Synonyms:benzyl [2-[(3S)-4-hydroxy-2,6-dimethylheptan-3-ylamino]-2-oxoethyl]carbamate

Chemical Property of benzyl [2-[(3S)-4-hydroxy-2,6-dimethylheptan-3-ylamino]-2-oxoethyl]carbamate

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Technology Process of benzyl [2-[(3S)-4-hydroxy-2,6-dimethylheptan-3-ylamino]-2-oxoethyl]carbamate

There total 1 articles about benzyl [2-[(3S)-4-hydroxy-2,6-dimethylheptan-3-ylamino]-2-oxoethyl]carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

tert-butyl [(3S)-4-hydroxy-2,6-dimethylheptan-3-yl]carbamate + N-(Benzyloxycarbonyl)glycine (1138-80-3) → benzyl [2-[(3S)-4-hydroxy-2,6-dimethylheptan-3-ylamino]-2-oxoethyl]carbamate (1596798-44-5)

Guidance literature:

tert-butyl [(3S)-4-hydroxy-2,6-dimethylheptan-3-yl]carbamate; With trifluoroacetic acid; In dichloromethane; Inert atmosphere;

N-(Benzyloxycarbonyl)glycine; With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In dichloromethane; Inert atmosphere;

DOI:10.1002/ejoc.201301435

Reference yield: 84.0%

benzyl [2-[(3S)-4-hydroxy-2,6-dimethylheptan-3-ylamino]-2-oxoethyl]carbamate (1596798-44-5) → (S)-benzyl [2-(2,6-dimethyl-4-oxoheptan-3-ylamino)-2-oxoethyl]-carbamate (1596798-56-9)

Guidance literature:

With Dess-Martin periodane; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;

DOI:10.1002/ejoc.201301435

Reference yield: 84.0%

benzyl [2-[(3S)-4-hydroxy-2,6-dimethylheptan-3-ylamino]-2-oxoethyl]carbamate (1596798-44-5) → (S)-benzyl [2-(2,6-dimethyl-4-oxoheptan-3-ylamino)-2-oxoethyl]-carbamate

Guidance literature:

With Dess-Martin periodane; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;

DOI:10.1002/ejoc.201301435

upstream raw materials:

N-(Benzyloxycarbonyl)glycine

Downstream raw materials:

(S)-benzyl [2-(2,6-dimethyl-4-oxoheptan-3-ylamino)-2-oxoethyl]-carbamate

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