8-iodo-6b,10b-dihydrobenzo[3,4]cyclobuta[1,2-a]acenaphthylene

Base Information

Chemical Name:8-iodo-6b,10b-dihydrobenzo[3,4]cyclobuta[1,2-a]acenaphthylene
CAS No.:219833-92-8
Molecular Formula:C₁₈H₁₁I
Molecular Weight:354.19
Hs Code.:
Mol file:219833-92-8.mol

Synonyms:8-iodo-6b,10b-dihydrobenzocyclobutacenaphthylene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 8-iodo-6b,10b-dihydrobenzo[3,4]cyclobuta[1,2-a]acenaphthylene

Chemical Property:

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Technology Process of 8-iodo-6b,10b-dihydrobenzo[3,4]cyclobuta[1,2-a]acenaphthylene

There total 1 articles about 8-iodo-6b,10b-dihydrobenzo[3,4]cyclobuta[1,2-a]acenaphthylene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5326-47-6
2-amino-5-iodobenzoic acid

: 208-96-8,25036-01-5
acenaphthylene

: 219833-92-8
8-iodo-6b,10b-dihydrobenzocyclobut acenaphthylene

Guidance literature:: With isopentyl nitrite; trichloroacetic acid; Yield given; Multistep reaction; 1.) THF, 0 deg C, 30 min; r.t., 2 h, 2.) CH₂ClCH₂Cl, r.t., overnight; 45 deg C, 2 d; 60 deg C, overnight;
DOI:10.1002/(SICI)1521-3765(19990104)5:1<289::AID-CHEM289>3.0.CO;2-1

Reference yield: 75.0%

: 100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6
styrene

: 219833-92-8
8-iodo-6b,10b-dihydrobenzocyclobut acenaphthylene

: 8-styryl-6b,10b-dihydrobenzocyclobut acenaphthylene

Guidance literature:: With palladium diacetate; triethylamine; In N,N-dimethyl-formamide; for 17h; Heating;
DOI:10.1021/jo981016z

Reference yield: 65.0%

: 150457-71-9
4-Vinylphthalonitrile

: 219833-92-8
8-iodo-6b,10b-dihydrobenzocyclobut acenaphthylene

: C₂₈H₁₆N₂

Guidance literature:: With tetrabutylammomium bromide; palladium diacetate; potassium carbonate; In N,N-dimethyl-formamide; at 100 ℃; for 3h; Inert atmosphere;
DOI:10.1142/S1088424613500879