benzyl 3,3'-anhydro-2,6-dideoxy-3-C-hydroxymethyl-β-D-ribo-hexopyranoside

Base Information

Chemical Name:benzyl 3,3'-anhydro-2,6-dideoxy-3-C-hydroxymethyl-β-D-ribo-hexopyranoside
CAS No.:108319-63-7
Molecular Formula:C₁₄H₁₈O₄
Molecular Weight:250.295
Hs Code.:

Synonyms:benzyl 3,3'-anhydro-2,6-dideoxy-3-C-hydroxymethyl-β-D-ribo-hexopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of benzyl 3,3'-anhydro-2,6-dideoxy-3-C-hydroxymethyl-β-D-ribo-hexopyranoside

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Technology Process of benzyl 3,3'-anhydro-2,6-dideoxy-3-C-hydroxymethyl-β-D-ribo-hexopyranoside

There total 5 articles about benzyl 3,3'-anhydro-2,6-dideoxy-3-C-hydroxymethyl-β-D-ribo-hexopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 108319-61-5
benzyl 3-C-methylen-2,3,6-trideoxy-β-D-erythro-hexopyranoside

: 108319-63-7
benzyl 3,3'-anhydro-2,6-dideoxy-3-C-hydroxymethyl-β-D-ribo-hexopyranoside

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; at 20 ℃; for 24h; stereoselective reaction;
DOI:10.1080/07328303.2017.1397682

Reference yield:

: 108319-59-1
Benzyl-4-O-benzoyl-2,6-didesoxy-β-D-erythro-hexopyranosid-3-ulose

: 108319-63-7
benzyl 3,3'-anhydro-2,6-dideoxy-3-C-hydroxymethyl-β-D-ribo-hexopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 46 percent

2: 83 percent / m-Cl-C₆H₄-CO₃H

With 3-chloro-benzenecarboperoxoic acid;

Reference yield:

: 113879-91-7
benzyl 4-O-benzoyl-2,6-dideoxy-β-L-arabino-hexopyranoside

: 108319-63-7
benzyl 3,3'-anhydro-2,6-dideoxy-3-C-hydroxymethyl-β-D-ribo-hexopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 75 percent / (C₆H₅N)2Cr₂O₇, CH₃COOH / CH₂Cl₂

2: 46 percent

3: 83 percent / m-Cl-C₆H₄-CO₃H

With (C₆H₅N)2Cr₂O₇; acetic acid; 3-chloro-benzenecarboperoxoic acid; In dichloromethane;