Technology Process of C23H28O5
There total 4 articles about C23H28O5 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C16H22O5;
With
di(n-butyl)tin oxide;
In
toluene;
at 110 ℃;
for 2h;
benzyl bromide;
With
tetra-(n-butyl)ammonium iodide;
In
toluene;
at 65 ℃;
for 14h;
regioselective reaction;
DOI:10.1021/ol501095w
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: toluene-4-sulfonic acid / 0.17 h / 20 °C
2.1: sodium hydride; 1H-imidazole / N,N-dimethyl-formamide / 0.25 h / 0 - 20 °C
2.2: 14 h / 20 °C
3.1: bismuth(III) chloride; water / acetonitrile / 14 h / 20 °C
4.1: di(n-butyl)tin oxide / toluene / 2 h / 110 °C
4.2: 14 h / 65 °C
With
1H-imidazole; bismuth(III) chloride; water; sodium hydride; di(n-butyl)tin oxide; toluene-4-sulfonic acid;
In
N,N-dimethyl-formamide; toluene; acetonitrile;
DOI:10.1021/ol501095w
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: bismuth(III) chloride; water / acetonitrile / 14 h / 20 °C
2.1: di(n-butyl)tin oxide / toluene / 2 h / 110 °C
2.2: 14 h / 65 °C
With
bismuth(III) chloride; water; di(n-butyl)tin oxide;
In
toluene; acetonitrile;
DOI:10.1021/ol501095w