1-[2-(2-methyl-5-nitro-imidazol-1-yl)ethyl]-4-(o-tolyloxymethyl)-1H-[1,2,3]triazole

Base Information

Chemical Name:1-[2-(2-methyl-5-nitro-imidazol-1-yl)ethyl]-4-(o-tolyloxymethyl)-1H-[1,2,3]triazole
CAS No.:1144040-20-9
Molecular Formula:C₁₆H₁₈N₆O₃
Molecular Weight:342.357
Hs Code.:

Synonyms:1-[2-(2-methyl-5-nitro-imidazol-1-yl)ethyl]-4-(o-tolyloxymethyl)-1H-[1,2,3]triazole

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Chemical Property of 1-[2-(2-methyl-5-nitro-imidazol-1-yl)ethyl]-4-(o-tolyloxymethyl)-1H-[1,2,3]triazole

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Technology Process of 1-[2-(2-methyl-5-nitro-imidazol-1-yl)ethyl]-4-(o-tolyloxymethyl)-1H-[1,2,3]triazole

There total 4 articles about 1-[2-(2-methyl-5-nitro-imidazol-1-yl)ethyl]-4-(o-tolyloxymethyl)-1H-[1,2,3]triazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 5652-20-0
1-methyl-2-(2-propynyloxy)benzene

: 60666-28-6
[2-(2-methyl-5-nitro-1H-imidazol-1-yl)]ethylazide

: 1144040-20-9
1-[2-(2-methyl-5-nitro-imidazol-1-yl)ethyl]-4-(o-tolyloxymethyl)-1H-[1,2,3]triazole

Guidance literature:: With copper(ll) sulfate pentahydrate; sodium L-ascorbate; In water; tert-butyl alcohol; at 20 ℃; for 2h;
DOI:10.1016/j.bmcl.2009.01.037

Reference yield:

: 95-48-7,77504-84-8
ortho-cresol

: 1144040-20-9
1-[2-(2-methyl-5-nitro-imidazol-1-yl)ethyl]-4-(o-tolyloxymethyl)-1H-[1,2,3]triazole

Guidance literature:: Multi-step reaction with 2 steps

1: Alkaline conditions

2: sodium L-ascorbate; copper(II) sulfate / tert-butyl alcohol; water / 2 h / 20 °C

With copper(II) sulfate; sodium L-ascorbate; In water; tert-butyl alcohol; 1: |Williamson Ether Synthesis;
DOI:10.1016/j.ejmech.2016.03.041

Reference yield:

: 30575-42-9
toluene-4-sulfonic acid 2-(2-methyl-5-nitro-1H-imidazol-1-yl)ethyl ester

: 1144040-20-9
1-[2-(2-methyl-5-nitro-imidazol-1-yl)ethyl]-4-(o-tolyloxymethyl)-1H-[1,2,3]triazole

Guidance literature:: Multi-step reaction with 2 steps

1: sodium azide / N,N-dimethyl-formamide / 1 h / 0 - 80 °C

2: sodium L-ascorbate; copper(II) sulfate / tert-butyl alcohol; water / 2 h / 20 °C

With sodium azide; copper(II) sulfate; sodium L-ascorbate; In water; N,N-dimethyl-formamide; tert-butyl alcohol;
DOI:10.1016/j.ejmech.2016.03.041