Allyl-[2-(tert-butyl-dimethyl-silanyloxy)-2-(3-methoxy-phenyl)-ethyl]-amine

Base Information

Chemical Name:Allyl-[2-(tert-butyl-dimethyl-silanyloxy)-2-(3-methoxy-phenyl)-ethyl]-amine
CAS No.:129416-03-1
Molecular Formula:C₁₈H₃₁NO₂Si
Molecular Weight:321.535
Hs Code.:

Synonyms:Allyl-[2-(tert-butyl-dimethyl-silanyloxy)-2-(3-methoxy-phenyl)-ethyl]-amine

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Chemical Property of Allyl-[2-(tert-butyl-dimethyl-silanyloxy)-2-(3-methoxy-phenyl)-ethyl]-amine

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Technology Process of Allyl-[2-(tert-butyl-dimethyl-silanyloxy)-2-(3-methoxy-phenyl)-ethyl]-amine

There total 6 articles about Allyl-[2-(tert-butyl-dimethyl-silanyloxy)-2-(3-methoxy-phenyl)-ethyl]-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 27382-18-9
2-amino-1-(3-methoxyphenyl)ethanol

: 129416-03-1
Allyl-[2-(tert-butyl-dimethyl-silanyloxy)-2-(3-methoxy-phenyl)-ethyl]-amine

Guidance literature:: Multi-step reaction with 4 steps

1: 93 percent / pyridine / CH₂Cl₂ / 0 °C

2: 90 percent / KH / tetrahydrofuran

3: 4 N NaOH / ethanol / Heating

4: DMAP, iPr₂NEt / CH₂Cl₂

With pyridine; dmap; sodium hydroxide; potassium hydride; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; ethanol; dichloromethane;
DOI:10.1016/0040-4039(90)80083-X

Reference yield:

: 129416-01-9
5-(3-Methoxy-phenyl)-oxazolidin-2-one

: 129416-03-1
Allyl-[2-(tert-butyl-dimethyl-silanyloxy)-2-(3-methoxy-phenyl)-ethyl]-amine

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / KH / tetrahydrofuran

2: 4 N NaOH / ethanol / Heating

3: DMAP, iPr₂NEt / CH₂Cl₂

With dmap; sodium hydroxide; potassium hydride; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; ethanol; dichloromethane;
DOI:10.1016/0040-4039(90)80083-X

Reference yield:

: 129416-00-8
(tert-Butyl-dimethyl-silanyloxy)-(3-methoxy-phenyl)-acetonitrile

: 129416-03-1
Allyl-[2-(tert-butyl-dimethyl-silanyloxy)-2-(3-methoxy-phenyl)-ethyl]-amine

Guidance literature:: Multi-step reaction with 5 steps

1: 96 percent / LiAlH₄ / diethyl ether / 0 °C

2: 93 percent / pyridine / CH₂Cl₂ / 0 °C

3: 90 percent / KH / tetrahydrofuran

4: 4 N NaOH / ethanol / Heating

5: DMAP, iPr₂NEt / CH₂Cl₂

With pyridine; dmap; sodium hydroxide; lithium aluminium tetrahydride; potassium hydride; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; diethyl ether; ethanol; dichloromethane;
DOI:10.1016/0040-4039(90)80083-X