C₃₈H₆₄SSiO₄H₂

Base Information

Chemical Name:C₃₈H₆₄SSiO₄H₂
CAS No.:947769-26-8
Molecular Formula:C₃₈H₆₆O₄SSi
Molecular Weight:647.091
Hs Code.:

C<sub>38</sub>H<sub>64</sub>SSiO<sub>4</sub>H<sub>2</sub>

Synonyms:C₃₈H₆₄SSiO₄H₂

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Chemical Property of C₃₈H₆₄SSiO₄H₂

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Technology Process of C₃₈H₆₄SSiO₄H₂

There total 10 articles about C₃₈H₆₄SSiO₄H₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 947769-20-2
C₃₈H₆₄SSiO₄

: 947769-26-8
C₃₈H₆₄SSiO₄H₂

: C₃₈H₆₄SSiO₄H₂

Guidance literature:: With lithium aluminium tetrahydride; lithium iodide; In diethyl ether; at -100 ℃; for 0.333333h;
DOI:10.1021/ol071024e

Reference yield:

: C₁₈H₃₅ISiO

: 947769-26-8
C₃₈H₆₄SSiO₄H₂

Guidance literature:: Multi-step reaction with 5 steps

1.1: 92 percent / Pd(PPh₃)4 / tetrahydrofuran / 14 h / 0 °C

2.1: DIBAL-H / CH₂Cl₂ / 3 h / -78 °C

3.1: 99 percent / CBr₄; 2,6-lutidine; PPh₃ / CH₂Cl₂ / 20 °C

4.1: t-BuLi / diethyl ether; pentane / 0.33 h / -78 - -40 °C

4.2: 72 mg / diethyl ether; pentane / 0.33 h / -78 °C

5.1: 87 percent / LiI; LiAlH₄ / diethyl ether / 0.33 h / -100 °C

With 2,6-dimethylpyridine; lithium aluminium tetrahydride; carbon tetrabromide; tert.-butyl lithium; diisobutylaluminium hydride; triphenylphosphine; lithium iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; diethyl ether; dichloromethane; pentane;
DOI:10.1021/ol071024e

Reference yield:

: 947769-16-6
C₂₂H₄₄SiO₂

: 947769-26-8
C₃₈H₆₄SSiO₄H₂

Guidance literature:: Multi-step reaction with 3 steps

1.1: 99 percent / CBr₄; 2,6-lutidine; PPh₃ / CH₂Cl₂ / 20 °C

2.1: t-BuLi / diethyl ether; pentane / 0.33 h / -78 - -40 °C

2.2: 72 mg / diethyl ether; pentane / 0.33 h / -78 °C

3.1: 87 percent / LiI; LiAlH₄ / diethyl ether / 0.33 h / -100 °C

With 2,6-dimethylpyridine; lithium aluminium tetrahydride; carbon tetrabromide; tert.-butyl lithium; triphenylphosphine; lithium iodide; In diethyl ether; dichloromethane; pentane;
DOI:10.1021/ol071024e