1-(1,2,3,6-tetrahydro-4-methyl-1-(4-methylphenyl)-sulfonyl-2-pyridinyl)-ethanone

Base Information

Chemical Name:1-(1,2,3,6-tetrahydro-4-methyl-1-(4-methylphenyl)-sulfonyl-2-pyridinyl)-ethanone
CAS No.:1147121-48-9
Molecular Formula:C₁₅H₁₉NO₃S
Molecular Weight:293.387
Hs Code.:

Synonyms:1-(1,2,3,6-tetrahydro-4-methyl-1-(4-methylphenyl)-sulfonyl-2-pyridinyl)-ethanone

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Chemical Property of 1-(1,2,3,6-tetrahydro-4-methyl-1-(4-methylphenyl)-sulfonyl-2-pyridinyl)-ethanone

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Technology Process of 1-(1,2,3,6-tetrahydro-4-methyl-1-(4-methylphenyl)-sulfonyl-2-pyridinyl)-ethanone

There total 1 articles about 1-(1,2,3,6-tetrahydro-4-methyl-1-(4-methylphenyl)-sulfonyl-2-pyridinyl)-ethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1147121-31-0
6-methyl-2-(1-methylethenyl)-4-[(4-methylphenyl)-sulfonyl]-3,4-dihydro-2H-1,4-oxazine

: 1147121-48-9
1-(1,2,3,6-tetrahydro-4-methyl-1-(4-methylphenyl)-sulfonyl-2-pyridinyl)-ethanone

Guidance literature:: In toluene; at 216 ℃; for 60h; Inert atmosphere; Sealed tube;
DOI:10.1016/j.tet.2009.01.065

Reference yield: 88.0%

: 1147121-48-9
1-(1,2,3,6-tetrahydro-4-methyl-1-(4-methylphenyl)-sulfonyl-2-pyridinyl)-ethanone

: 69739-34-0
t-butyldimethylsiyl triflate

: 13291-18-4
isopropenylmagnesium bromide

: C₂₄H₃₉NO₃SSi

Guidance literature:: 1-(1,2,3,6-tetrahydro-4-methyl-1-(4-methylphenyl)-sulfonyl-2-pyridinyl)-ethanone; isopropenylmagnesium bromide; In tetrahydrofuran; at 0 ℃;

t-butyldimethylsiyl triflate; With triethylamine; In dichloromethane; at -78 - 20 ℃;
DOI:10.1039/c7cc08511g

Reference yield: 71.0%

: 1147121-48-9
1-(1,2,3,6-tetrahydro-4-methyl-1-(4-methylphenyl)-sulfonyl-2-pyridinyl)-ethanone

: 69739-34-0
t-butyldimethylsiyl triflate

: 1826-67-1
vinyl magnesium bromide

: C₂₃H₃₇NO₃SSi

Guidance literature:: 1-(1,2,3,6-tetrahydro-4-methyl-1-(4-methylphenyl)-sulfonyl-2-pyridinyl)-ethanone; vinyl magnesium bromide; In tetrahydrofuran; at 0 ℃;

t-butyldimethylsiyl triflate; With triethylamine; In dichloromethane; at -78 - 20 ℃;
DOI:10.1039/c7cc08511g