Technology Process of C23H32O6
There total 4 articles about C23H32O6 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: 83 percent / diisobutylaluminum hydride / toluene / 3 h / 20 °C
2.1: oxalyl chloride; DMSO; Et3N / CH2Cl2 / 3 h / 0 °C
3.1: NaH2PO4; 2-methyl-2-butene; NaClO2 / 2-methyl-propan-2-ol; H2O / 2.5 h / 20 °C
4.1: 2,4,6-trichlorobenzoyl chloride; Et3N / toluene / 1.5 h
4.2: 764 mg / 4-dimethylaminopyridine / toluene / 2 h / 20 °C
5.1: 77 percent / first-generation ruthenium indenylidene complex / CH2Cl2 / 15 h / Heating
With
sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; oxalyl dichloride; 2,4,6-trichlorobenzoyl chloride; diisobutylaluminium hydride; dimethyl sulfoxide; triethylamine;
first-generation ruthenium indenylidene complex;
In
dichloromethane; water; toluene; tert-butyl alcohol;
DOI:10.1002/chem.200601370
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: oxalyl chloride; DMSO; Et3N / CH2Cl2 / 3 h / 0 °C
2.1: NaH2PO4; 2-methyl-2-butene; NaClO2 / 2-methyl-propan-2-ol; H2O / 2.5 h / 20 °C
3.1: 2,4,6-trichlorobenzoyl chloride; Et3N / toluene / 1.5 h
3.2: 764 mg / 4-dimethylaminopyridine / toluene / 2 h / 20 °C
4.1: 77 percent / first-generation ruthenium indenylidene complex / CH2Cl2 / 15 h / Heating
With
sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; oxalyl dichloride; 2,4,6-trichlorobenzoyl chloride; dimethyl sulfoxide; triethylamine;
first-generation ruthenium indenylidene complex;
In
dichloromethane; water; toluene; tert-butyl alcohol;
DOI:10.1002/chem.200601370
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: NaH2PO4; 2-methyl-2-butene; NaClO2 / 2-methyl-propan-2-ol; H2O / 2.5 h / 20 °C
2.1: 2,4,6-trichlorobenzoyl chloride; Et3N / toluene / 1.5 h
2.2: 764 mg / 4-dimethylaminopyridine / toluene / 2 h / 20 °C
3.1: 77 percent / first-generation ruthenium indenylidene complex / CH2Cl2 / 15 h / Heating
With
sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; 2,4,6-trichlorobenzoyl chloride; triethylamine;
first-generation ruthenium indenylidene complex;
In
dichloromethane; water; toluene; tert-butyl alcohol;
DOI:10.1002/chem.200601370