3-(4-chlorophenyl)-N-methyl-4-phenyl-4,5-dihydro-1H-pyrazole-1-carbothioamide

Base Information

Chemical Name:3-(4-chlorophenyl)-N-methyl-4-phenyl-4,5-dihydro-1H-pyrazole-1-carbothioamide
CAS No.:1207386-64-8
Molecular Formula:C₁₇H₁₆ClN₃S
Molecular Weight:329.853
Hs Code.:

Synonyms:3-(4-chlorophenyl)-N-methyl-4-phenyl-4,5-dihydro-1H-pyrazole-1-carbothioamide

Suppliers and Price of 3-(4-chlorophenyl)-N-methyl-4-phenyl-4,5-dihydro-1H-pyrazole-1-carbothioamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-(4-chlorophenyl)-N-methyl-4-phenyl-4,5-dihydro-1H-pyrazole-1-carbothioamide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 3-(4-chlorophenyl)-N-methyl-4-phenyl-4,5-dihydro-1H-pyrazole-1-carbothioamide

There total 1 articles about 3-(4-chlorophenyl)-N-methyl-4-phenyl-4,5-dihydro-1H-pyrazole-1-carbothioamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 556-61-6
methyl thioisocyanate

: 59074-26-9
3-(4-chlorophenyl)-4-phenyl-4,5-dihydro-1H-pyrazole

: 1207386-64-8
3-(4-chlorophenyl)-N-methyl-4-phenyl-4,5-dihydro-1H-pyrazole-1-carbothioamide

Guidance literature:: In ethanol; for 3h; Inert atmosphere; Reflux;

Reference yield: 100.0%

: 1207386-64-8
3-(4-chlorophenyl)-N-methyl-4-phenyl-4,5-dihydro-1H-pyrazole-1-carbothioamide

: 74-88-4
methyl iodide

: 1207386-65-9
methyl 3-(4-chlorophenyl)-N-methyl-4-phenyl-4,5-dihydro-1H-pyrazole-1-carbothioimidate

Guidance literature:: In methanol; at 40 ℃; Product distribution / selectivity; Inert atmosphere;

Reference yield:

: 1207386-64-8
3-(4-chlorophenyl)-N-methyl-4-phenyl-4,5-dihydro-1H-pyrazole-1-carbothioamide

: 362519-49-1
3-(4-chlorophenyl)-N'-[(4-chlorophenyl)sulfonyl]-N-methyl-4-phenyl-4,5-dihydro-1H-pyrazole-1-carboxamidine

Guidance literature:: Multi-step reaction with 2 steps

1: methanol / 16 h / 40 °C / Inert atmosphere

2: acetonitrile / 16 h / Reflux

In methanol; acetonitrile;
DOI:10.1016/j.tetlet.2011.01.068