N₁,N₃-bis(3-phenyl-3,4-dihydro-2H-benzo[e][1,3]oxazin-6-yl)isophthalamide

Base Information

Chemical Name:N₁,N₃-bis(3-phenyl-3,4-dihydro-2H-benzo[e][1,3]oxazin-6-yl)isophthalamide
CAS No.:1217505-00-4
Molecular Formula:C₃₆H₃₀N₄O₄
Molecular Weight:582.659
Hs Code.:

N<sub>1</sub>,N<sub>3</sub>-bis(3-phenyl-3,4-dihydro-2H-benzo[e][1,3]oxazin-6-yl)isophthalamide

Synonyms:N₁,N₃-bis(3-phenyl-3,4-dihydro-2H-benzo[e][1,3]oxazin-6-yl)isophthalamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N₁,N₃-bis(3-phenyl-3,4-dihydro-2H-benzo[e][1,3]oxazin-6-yl)isophthalamide

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Technology Process of N₁,N₃-bis(3-phenyl-3,4-dihydro-2H-benzo[e][1,3]oxazin-6-yl)isophthalamide

There total 4 articles about N₁,N₃-bis(3-phenyl-3,4-dihydro-2H-benzo[e][1,3]oxazin-6-yl)isophthalamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 395676-99-0
3-phenyl-3,4-dihydro-2H-benzo[e][1,3]oxazin-6-amine

: 99-63-8
benzene-1,3-dicarbonyl dichloride

: 1217505-00-4
N₁,N₃-bis(3-phenyl-3,4-dihydro-2H-benzo[e][1,3]oxazin-6-yl)isophthalamide

Guidance literature:: With triethylamine; In chloroform; for 1h; Cooling with ice;
DOI:10.1021/ma902556k

Reference yield:

: 1217504-95-4
4,5,6,7-tetrachloro-2-(3-phenyl-3,4-dihydro-2H-benzo[e][1,3]oxazin-6-yl)isoindoline-1,3-dione

: 1217505-00-4
N₁,N₃-bis(3-phenyl-3,4-dihydro-2H-benzo[e][1,3]oxazin-6-yl)isophthalamide

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogen; hydrazine hydrate / diethyl ether / 5 h / Cooling with ice

2: triethylamine / chloroform / 1 h / Cooling with ice

With hydrogen; hydrazine hydrate; triethylamine; In diethyl ether; chloroform;
DOI:10.1021/ma902556k

Reference yield:

: 1217504-98-7
2,2,2-trifluoro-N-(3-phenyl-3,4-dihydro-2H-benzo[e][1,3]oxazin-6-yl)acetamide

: 1217505-00-4
N₁,N₃-bis(3-phenyl-3,4-dihydro-2H-benzo[e][1,3]oxazin-6-yl)isophthalamide

Guidance literature:: Multi-step reaction with 2 steps

1: sodium tetrahydroborate / methanol; ethyl acetate / 6 h / 20 °C / Inert atmosphere

2: triethylamine / chloroform / 1 h / Cooling with ice

With sodium tetrahydroborate; triethylamine; In methanol; chloroform; ethyl acetate;
DOI:10.1021/ma902556k