4,5,6,7-tetrachloro-2-(3-phenyl-3,4-dihydro-2H-benzo[e][1,3]oxazin-6-yl)isoindoline-1,3-dione

Base Information

Chemical Name:4,5,6,7-tetrachloro-2-(3-phenyl-3,4-dihydro-2H-benzo[e][1,3]oxazin-6-yl)isoindoline-1,3-dione
CAS No.:1217504-95-4
Molecular Formula:C₂₂H₁₂Cl₄N₂O₃
Molecular Weight:494.161
Hs Code.:

Synonyms:4,5,6,7-tetrachloro-2-(3-phenyl-3,4-dihydro-2H-benzo[e][1,3]oxazin-6-yl)isoindoline-1,3-dione

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Chemical Property of 4,5,6,7-tetrachloro-2-(3-phenyl-3,4-dihydro-2H-benzo[e][1,3]oxazin-6-yl)isoindoline-1,3-dione

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Technology Process of 4,5,6,7-tetrachloro-2-(3-phenyl-3,4-dihydro-2H-benzo[e][1,3]oxazin-6-yl)isoindoline-1,3-dione

There total 1 articles about 4,5,6,7-tetrachloro-2-(3-phenyl-3,4-dihydro-2H-benzo[e][1,3]oxazin-6-yl)isoindoline-1,3-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 41406-65-9
4,5,6,7-tetrachloro-2-(4-hydroxyphenyl)-isoindoline-1,3-dione

: 62-53-3
aniline

: 1217504-95-4
4,5,6,7-tetrachloro-2-(3-phenyl-3,4-dihydro-2H-benzo[e][1,3]oxazin-6-yl)isoindoline-1,3-dione

Guidance literature:: In xylenes; at 120 ℃; for 36h;
DOI:10.1021/ma902556k

Reference yield: 80.0%

: 1217504-95-4
4,5,6,7-tetrachloro-2-(3-phenyl-3,4-dihydro-2H-benzo[e][1,3]oxazin-6-yl)isoindoline-1,3-dione

: 395676-99-0
3-phenyl-3,4-dihydro-2H-benzo[e][1,3]oxazin-6-amine

Guidance literature:: With hydrogen; hydrazine hydrate; In diethyl ether; for 5h; Cooling with ice;
DOI:10.1021/ma902556k

Reference yield:

: 1217504-95-4
4,5,6,7-tetrachloro-2-(3-phenyl-3,4-dihydro-2H-benzo[e][1,3]oxazin-6-yl)isoindoline-1,3-dione

: 1217505-00-4
N₁,N₃-bis(3-phenyl-3,4-dihydro-2H-benzo[e][1,3]oxazin-6-yl)isophthalamide

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogen; hydrazine hydrate / diethyl ether / 5 h / Cooling with ice

2: triethylamine / chloroform / 1 h / Cooling with ice

With hydrogen; hydrazine hydrate; triethylamine; In diethyl ether; chloroform;
DOI:10.1021/ma902556k