Phosphoramidothioic acid, O,O-bis(p-chlorophenyl) ester

Base Information

Chemical Name:Phosphoramidothioic acid, O,O-bis(p-chlorophenyl) ester
CAS No.:15045-55-3
Molecular Formula:C₁₂H₁₀Cl₂NO₂PS
Molecular Weight:334.163
Hs Code.:2931900090
NSC Number:202878
DSSTox Substance ID:DTXSID40164554
Nikkaji Number:J50.354A
Mol file:15045-55-3.mol

Synonyms:15045-55-3;O,O-Bis(p-chlorophenyl)phosphoramidothioate;Phosphoramidothioic acid, O,O-bis(p-chlorophenyl) ester;1-[amino-(4-chlorophenoxy)phosphinothioyl]oxy-4-chlorobenzene;Phosphoramidothioic acid O,O-bis(p-chlorophenyl) ester;NSC 202878;BRN 2146745;NSC202878;WLN: GR DOPZS&OR DG;1-06-00-00102 (Beilstein Handbook Reference);DTXSID40164554;NSC-202878;Phosphoramidothioic acid,O-bis(p-chlorophenyl) ester

Suppliers and Price of Phosphoramidothioic acid, O,O-bis(p-chlorophenyl) ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of Phosphoramidothioic acid, O,O-bis(p-chlorophenyl) ester

Chemical Property:

Vapor Pressure:9.62E-08mmHg at 25°C
Boiling Point:434.2°C at 760 mmHg
Flash Point:216.4°C
PSA：86.38000
Density:1.485g/cm³
LogP:5.98530
XLogP3:4.1
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:4
Exact Mass:332.9546921
Heavy Atom Count:19
Complexity:304

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC(=CC=C1OP(=S)(N)OC2=CC=C(C=C2)Cl)Cl

Technology Process of Phosphoramidothioic acid, O,O-bis(p-chlorophenyl) ester

There total 4 articles about Phosphoramidothioic acid, O,O-bis(p-chlorophenyl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 55526-70-0
bis(4-chlorophenyl) chlorothiophosphate

: 15045-55-3
amidothiophosphoric acid O,O'-bis-(4-chloro-phenyl ester)

Guidance literature:: With ammonia; In benzene; at 40 ℃; for 2h;
DOI:10.1080/104265090968064

Reference yield:

: 106-48-9,82344-39-6
4-chloro-phenol

: 15045-55-3
amidothiophosphoric acid O,O'-bis-(4-chloro-phenyl ester)

Guidance literature:: Multi-step reaction with 2 steps

1: 78.2 percent / thiophosphyl chloride; aq. sodium hydroxide; benzyltriethylammonium chloride / benzene

2: ammonia / benzene / 2 h / 40 °C

With trichlorothiophosphine; sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride; ammonia; In benzene;
DOI:10.1080/104265090968064