(S)-tert-butyl 2-(3-phenyl-1,2,4-oxadiazol-5-yl)pyrrolidine-1-carboxylate

Base Information

Chemical Name:(S)-tert-butyl 2-(3-phenyl-1,2,4-oxadiazol-5-yl)pyrrolidine-1-carboxylate
CAS No.:336784-56-6
Molecular Formula:C₁₇H₂₁N₃O₃
Molecular Weight:315.372
Hs Code.:

Synonyms:(S)-tert-butyl 2-(3-phenyl-1,2,4-oxadiazol-5-yl)pyrrolidine-1-carboxylate

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Chemical Property of (S)-tert-butyl 2-(3-phenyl-1,2,4-oxadiazol-5-yl)pyrrolidine-1-carboxylate

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Technology Process of (S)-tert-butyl 2-(3-phenyl-1,2,4-oxadiazol-5-yl)pyrrolidine-1-carboxylate

There total 9 articles about (S)-tert-butyl 2-(3-phenyl-1,2,4-oxadiazol-5-yl)pyrrolidine-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 15761-39-4,59433-50-0
1-(tert-butoxycarbonyl)-L-proline

: 613-92-3
N-hydroxybenzenecarboximidamide

: 336784-56-6
(S)-tert-butyl 2-(3-phenyl-1,2,4-oxadiazol-5-yl)pyrrolidine-1-carboxylate

Guidance literature:: 1-(tert-butoxycarbonyl)-L-proline; N-hydroxybenzenecarboximidamide; With 1-hydroxy-7-aza-benzotriazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 20 ℃;

In 1,4-dioxane; at 100 ℃;
DOI:10.1016/j.ejmech.2020.112100

Reference yield:

: 15761-39-4,59433-50-0
1-(tert-butoxycarbonyl)-L-proline

: 613-92-3
N-hydroxybenzamidine

: 336784-56-6
(S)-tert-butyl 2-(3-phenyl-1,2,4-oxadiazol-5-yl)pyrrolidine-1-carboxylate

Guidance literature:: 1-(tert-butoxycarbonyl)-L-proline; N-hydroxybenzamidine; With diisopropyl-carbodiimide; In dichloromethane; at 20 ℃; for 12h;

In pyridine; dichloromethane; for 10h; Heating / reflux;