2-Acetylamino-acrylic acid (3S,4R)-2-isopropyl-5-(S)-methyl-cyclohexyl ester

Base Information

Chemical Name:2-Acetylamino-acrylic acid (3S,4R)-2-isopropyl-5-(S)-methyl-cyclohexyl ester
CAS No.:145644-80-0
Molecular Formula:C₁₅H₂₅NO₃
Molecular Weight:267.368
Hs Code.:

Synonyms:2-Acetylamino-acrylic acid (3S,4R)-2-isopropyl-5-(S)-methyl-cyclohexyl ester

Suppliers and Price of 2-Acetylamino-acrylic acid (3S,4R)-2-isopropyl-5-(S)-methyl-cyclohexyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2-Acetylamino-acrylic acid (3S,4R)-2-isopropyl-5-(S)-methyl-cyclohexyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2-Acetylamino-acrylic acid (3S,4R)-2-isopropyl-5-(S)-methyl-cyclohexyl ester

There total 1 articles about 2-Acetylamino-acrylic acid (3S,4R)-2-isopropyl-5-(S)-methyl-cyclohexyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 35356-70-8
Methyl 2-acetamidoacrylate

: 2216-51-5
(-)-menthol

: 145644-80-0
2-Acetylamino-acrylic acid (3S,4R)-2-isopropyl-5-(S)-methyl-cyclohexyl ester

Guidance literature:: With trimethylaluminum; Yield given. Multistep reaction; 1.) hexane, toluene, room temp., 20 min, 2.) 60 deg C, 8h;
DOI:10.1055/s-1990-26828

Reference yield: 52.0%

: 145644-80-0
2-Acetylamino-acrylic acid (3S,4R)-2-isopropyl-5-(S)-methyl-cyclohexyl ester

: 106-99-0,130983-70-9,29406-96-0,9003-17-2
buta-1,3-diene

: (1'S,2'R,5'S)-menthyl 1-acetamido-3-cyclohexene-1-carboxylate

Guidance literature:: With titanium tetrachloride; In dichloromethane; at 0 ℃; for 216h;
DOI:10.1016/0957-4166(96)00067-5

Reference yield:

: 145644-80-0
2-Acetylamino-acrylic acid (3S,4R)-2-isopropyl-5-(S)-methyl-cyclohexyl ester

: phenylmagnesium bromide

: (1S,2R,5S)-menthyl (2R)-acetamido-3-phenylpropanoate

: (1S,2R,5S)-menthyl (2S)-acetamido-3-phenylpropanoate

Guidance literature:: With copper(l) iodide; ammonium chloride; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts; 1.) Et₂O, 0 deg C, 1 h, 2.) -80 deg C (5 min) to room temperature;
DOI:10.1139/v92-294