N¹,N⁵,N¹⁰,N¹⁴-tetra(p-toluenesulfonyl)-1,14-diamino-5,10-diazatetradecane

Base Information

Chemical Name:N¹,N⁵,N¹⁰,N¹⁴-tetra(p-toluenesulfonyl)-1,14-diamino-5,10-diazatetradecane
CAS No.:277760-01-7
Molecular Formula:C₄₀H₅₄N₄O₈S₄
Molecular Weight:847.155
Hs Code.:

N<sup>1</sup>,N<sup>5</sup>,N<sup>10</sup>,N<sup>14</sup>-tetra(p-toluenesulfonyl)-1,14-diamino-5,10-diazatetradecane

Synonyms:N¹,N⁵,N¹⁰,N¹⁴-tetra(p-toluenesulfonyl)-1,14-diamino-5,10-diazatetradecane

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Chemical Property of N¹,N⁵,N¹⁰,N¹⁴-tetra(p-toluenesulfonyl)-1,14-diamino-5,10-diazatetradecane

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Technology Process of N¹,N⁵,N¹⁰,N¹⁴-tetra(p-toluenesulfonyl)-1,14-diamino-5,10-diazatetradecane

There total 5 articles about N¹,N⁵,N¹⁰,N¹⁴-tetra(p-toluenesulfonyl)-1,14-diamino-5,10-diazatetradecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 98-59-9
p-toluenesulfonyl chloride

: 278807-13-9
C₂₈H₄₂N₄O₆S₂

: 277760-01-7
N¹,N⁵,N¹⁰,N¹⁴-tetra(p-toluenesulfonyl)-1,14-diamino-5,10-diazatetradecane

Guidance literature:: C₂₈H₄₂N₄O₆S₂; With hydrogenchloride; at 70 ℃; for 1h;

p-toluenesulfonyl chloride; With triethylamine; In pyridine; at 20 ℃; for 4h;
DOI:10.1016/S0968-0896(00)00156-5

Reference yield:

: 5394-18-3
2-(4-bromobutyl)isoindoline-1,3-dione

: 277760-01-7
N¹,N⁵,N¹⁰,N¹⁴-tetra(p-toluenesulfonyl)-1,14-diamino-5,10-diazatetradecane

Guidance literature:: Multi-step reaction with 3 steps

2.1: N₂H₄ / dimethylformamide / 24 h / 70 °C

3.1: 1.2 M HCl / 1 h / 70 °C

3.2: Et₃N / pyridine / 4 h / 20 °C

With hydrogenchloride; hydrazine; In N,N-dimethyl-formamide; 1.1: Alkylation / 2.1: Reduction / 3.1: decarbonylation / 3.2: Tosylation;
DOI:10.1016/S0968-0896(00)00156-5

Reference yield:

: 15544-47-5
N,N'-ditosyl-1,4-diaminobutane

: 277760-01-7
N¹,N⁵,N¹⁰,N¹⁴-tetra(p-toluenesulfonyl)-1,14-diamino-5,10-diazatetradecane

Guidance literature:: Multi-step reaction with 3 steps

2.1: N₂H₄ / dimethylformamide / 24 h / 70 °C

3.1: 1.2 M HCl / 1 h / 70 °C

3.2: Et₃N / pyridine / 4 h / 20 °C

With hydrogenchloride; hydrazine; In N,N-dimethyl-formamide; 1.1: Alkylation / 2.1: Reduction / 3.1: decarbonylation / 3.2: Tosylation;
DOI:10.1016/S0968-0896(00)00156-5