4-[(1R,2R,3R,4S)-3-((Z)-6-Carboxy-hex-2-enyl)-bicyclo[2.2.1]hept-2-ylsulfamoyl]-benzoic acid

Base Information

• Chemical Name: 4-[(1R,2R,3R,4S)-3-((Z)-6-Carboxy-hex-2-enyl)-bicyclo[2.2.1]hept-2-ylsulfamoyl]-benzoic acid
• CAS No.: 115267-05-5
• Molecular Formula: C₂₁H₂₇NO₆S
• Molecular Weight: 421.514

Synonyms:4-[(1R,2R,3R,4S)-3-((Z)-6-Carboxy-hex-2-enyl)-bicyclo[2.2.1]hept-2-ylsulfamoyl]-benzoic acid

Chemical Property of 4-[(1R,2R,3R,4S)-3-((Z)-6-Carboxy-hex-2-enyl)-bicyclo[2.2.1]hept-2-ylsulfamoyl]-benzoic acid

Chemical Property:

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Technology Process of 4-[(1R,2R,3R,4S)-3-((Z)-6-Carboxy-hex-2-enyl)-bicyclo[2.2.1]hept-2-ylsulfamoyl]-benzoic acid

There total 1 articles about 4-[(1R,2R,3R,4S)-3-((Z)-6-Carboxy-hex-2-enyl)-bicyclo[2.2.1]hept-2-ylsulfamoyl]-benzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-[(1R,2R,3R,4S)-3-((Z)-6-Methoxycarbonyl-hex-2-enyl)-bicyclo[2.2.1]hept-2-ylsulfamoyl]-benzoic acid (115266-90-5) → 4-[(1R,2R,3R,4S)-3-((Z)-6-Carboxy-hex-2-enyl)-bicyclo[2.2.1]hept-2-ylsulfamoyl]-benzoic acid (115267-05-5)

Guidance literature:

With potassium hydroxide; In methanol; at 23 ℃; for 6h;

DOI:10.1021/jm00117a028

Reference yield: 25.0%

4-[(1R,2R,3R,4S)-3-((Z)-6-Carboxy-hex-2-enyl)-bicyclo[2.2.1]hept-2-ylsulfamoyl]-benzoic acid (115267-05-5) → C21H25NO6S(2-)*2Na(1+) (115303-23-6)

Guidance literature:

With sodium methylate; In methanol;

DOI:10.1021/jm00117a028

upstream raw materials:

4-[(1R,2R,3R,4S)-3-((Z)-6-Methoxycarbonyl-hex-2-enyl)-bicyclo[2.2.1]hept-2-ylsulfamoyl]-benzoic acid

Downstream raw materials:

C₂₁H₂₅NO₆S^(2-)*2Na⁽¹⁺⁾

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