4-[(1R,2R,3R,4S)-3-((Z)-6-Methoxycarbonyl-hex-2-enyl)-bicyclo[2.2.1]hept-2-ylsulfamoyl]-benzoic acid

Base Information

Chemical Name:4-[(1R,2R,3R,4S)-3-((Z)-6-Methoxycarbonyl-hex-2-enyl)-bicyclo[2.2.1]hept-2-ylsulfamoyl]-benzoic acid
CAS No.:115266-90-5
Molecular Formula:C₂₂H₂₉NO₆S
Molecular Weight:435.541
Hs Code.:

Synonyms:4-[(1R,2R,3R,4S)-3-((Z)-6-Methoxycarbonyl-hex-2-enyl)-bicyclo[2.2.1]hept-2-ylsulfamoyl]-benzoic acid

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Chemical Property of 4-[(1R,2R,3R,4S)-3-((Z)-6-Methoxycarbonyl-hex-2-enyl)-bicyclo[2.2.1]hept-2-ylsulfamoyl]-benzoic acid

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Technology Process of 4-[(1R,2R,3R,4S)-3-((Z)-6-Methoxycarbonyl-hex-2-enyl)-bicyclo[2.2.1]hept-2-ylsulfamoyl]-benzoic acid

There total 1 articles about 4-[(1R,2R,3R,4S)-3-((Z)-6-Methoxycarbonyl-hex-2-enyl)-bicyclo[2.2.1]hept-2-ylsulfamoyl]-benzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 23.0%

: 10130-89-9
p-carboxyphenylsulfonyl chloride

: 115266-76-7
(5Z)-7-<3-endo-aminobicyclo<2.2.1>hept-2-exo-yl>heptenoic acid methyl ester trifluoroacetate

: 115266-90-5
4-[(1R,2R,3R,4S)-3-((Z)-6-Methoxycarbonyl-hex-2-enyl)-bicyclo[2.2.1]hept-2-ylsulfamoyl]-benzoic acid

Guidance literature:: With triethylamine; In dichloromethane;
DOI:10.1021/jm00117a028

Reference yield:

: 115266-90-5
4-[(1R,2R,3R,4S)-3-((Z)-6-Methoxycarbonyl-hex-2-enyl)-bicyclo[2.2.1]hept-2-ylsulfamoyl]-benzoic acid

: 115267-05-5
4-[(1R,2R,3R,4S)-3-((Z)-6-Carboxy-hex-2-enyl)-bicyclo[2.2.1]hept-2-ylsulfamoyl]-benzoic acid

Guidance literature:: With potassium hydroxide; In methanol; at 23 ℃; for 6h;
DOI:10.1021/jm00117a028

Reference yield:

: 115266-90-5
4-[(1R,2R,3R,4S)-3-((Z)-6-Methoxycarbonyl-hex-2-enyl)-bicyclo[2.2.1]hept-2-ylsulfamoyl]-benzoic acid

: 115303-23-6
C₂₁H₂₅NO₆S^(2-)*2Na⁽¹⁺⁾

Guidance literature:: Multi-step reaction with 2 steps

1: 1 N KOH / methanol / 6 h / 23 °C

2: 25 percent / sodium methoxide / methanol

With potassium hydroxide; sodium methylate; In methanol;
DOI:10.1021/jm00117a028