5-(4,6-dimethoxy-1H-pyrazolo[3,4-d]pyrimidin-3-yl)pentyl dibenzyl phosphate

Base Information

Chemical Name:5-(4,6-dimethoxy-1H-pyrazolo[3,4-d]pyrimidin-3-yl)pentyl dibenzyl phosphate
CAS No.:952410-54-7
Molecular Formula:C₂₆H₃₁N₄O₆P
Molecular Weight:526.529
Hs Code.:

Synonyms:5-(4,6-dimethoxy-1H-pyrazolo[3,4-d]pyrimidin-3-yl)pentyl dibenzyl phosphate

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Chemical Property of 5-(4,6-dimethoxy-1H-pyrazolo[3,4-d]pyrimidin-3-yl)pentyl dibenzyl phosphate

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Technology Process of 5-(4,6-dimethoxy-1H-pyrazolo[3,4-d]pyrimidin-3-yl)pentyl dibenzyl phosphate

There total 4 articles about 5-(4,6-dimethoxy-1H-pyrazolo[3,4-d]pyrimidin-3-yl)pentyl dibenzyl phosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.5%

: 952410-51-4
6-(6-chloro-2,4-dimethoxypyrimidin-5-yl)-6-oxohexanyl dibenzyl phosphate

: 952410-54-7
5-(4,6-dimethoxy-1H-pyrazolo[3,4-d]pyrimidin-3-yl)pentyl dibenzyl phosphate

Guidance literature:: With hydrazine; In methanol; at 45 ℃; for 12h;
DOI:10.1021/jo070982r

Reference yield:

: 952410-48-9
ethyl 6-[bis(benzyloxy)phosphoryloxy]hexanoate

: 952410-54-7
5-(4,6-dimethoxy-1H-pyrazolo[3,4-d]pyrimidin-3-yl)pentyl dibenzyl phosphate

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-BuLi / tetrahydrofuran; hexane / 0.5 h / -78 °C

1.2: 26 percent / tetrahydrofuran / -78 - -40 °C

2.1: 61.5 percent / hydrazine / methanol / 12 h / 45 °C

With n-butyllithium; hydrazine; In tetrahydrofuran; methanol; hexane;
DOI:10.1021/jo070982r

Reference yield:

: 50651-75-7
silver dibenzylphosphate

: 952410-54-7
5-(4,6-dimethoxy-1H-pyrazolo[3,4-d]pyrimidin-3-yl)pentyl dibenzyl phosphate

Guidance literature:: Multi-step reaction with 3 steps

1.1: 79.2 percent / toluene / 24 h / Heating

2.1: n-BuLi / tetrahydrofuran; hexane / 0.5 h / -78 °C

2.2: 26 percent / tetrahydrofuran / -78 - -40 °C

3.1: 61.5 percent / hydrazine / methanol / 12 h / 45 °C

With n-butyllithium; hydrazine; In tetrahydrofuran; methanol; hexane; toluene;
DOI:10.1021/jo070982r