6-(6-chloro-2,4-dimethoxypyrimidin-5-yl)-6-oxohexanyl dibenzyl phosphate

Base Information

Chemical Name:6-(6-chloro-2,4-dimethoxypyrimidin-5-yl)-6-oxohexanyl dibenzyl phosphate
CAS No.:952410-51-4
Molecular Formula:C₂₆H₃₀ClN₂O₇P
Molecular Weight:548.96
Hs Code.:

Synonyms:6-(6-chloro-2,4-dimethoxypyrimidin-5-yl)-6-oxohexanyl dibenzyl phosphate

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Chemical Property of 6-(6-chloro-2,4-dimethoxypyrimidin-5-yl)-6-oxohexanyl dibenzyl phosphate

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Technology Process of 6-(6-chloro-2,4-dimethoxypyrimidin-5-yl)-6-oxohexanyl dibenzyl phosphate

There total 3 articles about 6-(6-chloro-2,4-dimethoxypyrimidin-5-yl)-6-oxohexanyl dibenzyl phosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 26.0%

: 952410-48-9
ethyl 6-[bis(benzyloxy)phosphoryloxy]hexanoate

: 6320-15-6
6-chloro-2,4-dimethoxypyrimidine

: 952410-51-4
6-(6-chloro-2,4-dimethoxypyrimidin-5-yl)-6-oxohexanyl dibenzyl phosphate

Guidance literature:: 6-chloro-2,4-dimethoxypyrimidine; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 0.5h;

ethyl 6-[bis(benzyloxy)phosphoryloxy]hexanoate; In tetrahydrofuran; at -78 - -40 ℃; Further stages.;
DOI:10.1021/jo070982r

Reference yield:

: 50651-75-7
silver dibenzylphosphate

: 952410-51-4
6-(6-chloro-2,4-dimethoxypyrimidin-5-yl)-6-oxohexanyl dibenzyl phosphate

Guidance literature:: Multi-step reaction with 2 steps

1.1: 79.2 percent / toluene / 24 h / Heating

2.1: n-BuLi / tetrahydrofuran; hexane / 0.5 h / -78 °C

2.2: 26 percent / tetrahydrofuran / -78 - -40 °C

With n-butyllithium; In tetrahydrofuran; hexane; toluene;
DOI:10.1021/jo070982r

Reference yield:

: 25542-62-5
6-bromo-hexanoic acid ethyl ester

: 952410-51-4
6-(6-chloro-2,4-dimethoxypyrimidin-5-yl)-6-oxohexanyl dibenzyl phosphate

Guidance literature:: Multi-step reaction with 2 steps

1.1: 79.2 percent / toluene / 24 h / Heating

2.1: n-BuLi / tetrahydrofuran; hexane / 0.5 h / -78 °C

2.2: 26 percent / tetrahydrofuran / -78 - -40 °C

With n-butyllithium; In tetrahydrofuran; hexane; toluene;
DOI:10.1021/jo070982r