C₃₆H₃₈O₁₀

Base Information

Chemical Name:C₃₆H₃₈O₁₀
CAS No.:273926-82-2
Molecular Formula:C₃₆H₃₈O₁₀
Molecular Weight:630.692
Hs Code.:

C<sub>36</sub>H<sub>38</sub>O<sub>10</sub>

Synonyms:C₃₆H₃₈O₁₀

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Chemical Property of C₃₆H₃₈O₁₀

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Technology Process of C₃₆H₃₈O₁₀

There total 12 articles about C₃₆H₃₈O₁₀ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 273926-75-3
C₃₆H₄₀O₁₀

: 273926-82-2
C₃₆H₃₈O₁₀

Guidance literature:: With tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide; In dichloromethane; at 20 ℃; for 3h;
DOI:10.1016/S0040-4020(00)00073-9

Reference yield:

: 13452-36-3
2,9,10-triacetyl-5-O-cinnamoyltaxicin-I

: 273926-82-2
C₃₆H₃₈O₁₀

Guidance literature:: Multi-step reaction with 12 steps

1.1: 70 percent / NH₂OH*HCl; NaOAc / ethanol; H₂O / 24 h / 80 °C

2.1: 81 percent / pyridine / 0.67 h / 20 °C

3.1: 81 percent / NaOMe / CH₂Cl₂; methanol / 24 h / 0 °C

4.1: 88 percent / pyridine / CH₂Cl₂ / 0.5 h / 0 °C

5.1: 100 percent / TBAF / tetrahydrofuran / 1 h / 20 °C

6.1: 83 percent / OsO₄; N-methylmorpholine N-oxide / tetrahydrofuran; H₂O; 2-methyl-propan-2-ol / 20 h / 20 °C

7.1: 95 percent / imidazole / dimethylformamide / 3 h / 20 °C

8.1: 83 percent / pyridine / 20 h / 20 °C

9.1: TBAF / tetrahydrofuran / 1 h / 20 °C

9.2: 76 percent / TBAOAc / butan-2-one / 20 h / Heating

10.1: 93 percent / DMAP / CH₂Cl₂ / 5 h / 20 °C

11.1: 64 percent / tetrahydrofuran; cyclohexane; diethyl ether / 0.33 h / -78 °C

12.1: 70 percent / n-methylmorpholine N-oxide; tetrapropylammonium perruthenate / CH₂Cl₂ / 3 h / 20 °C

With pyridine; 1H-imidazole; dmap; osmium(VIII) oxide; tetrapropylammonium perruthennate; hydroxylamine hydrochloride; tetrabutyl ammonium fluoride; sodium methylate; sodium acetate; 4-methylmorpholine N-oxide; In tetrahydrofuran; methanol; diethyl ether; ethanol; dichloromethane; cyclohexane; water; N,N-dimethyl-formamide; tert-butyl alcohol; 1.1: Hydrolysis / 2.1: silylation / 3.1: Deacetylation / 4.1: Carbonylation / 5.1: desilylation / 6.1: Oxidation / 7.1: silylation / 8.1: mesylation / 9.1: desylilation / 9.2: Cyclization / 10.1: Acetylation / 11.1: Phenylation / 12.1: Oxidation;
DOI:10.1016/S0040-4020(00)00073-9

Reference yield:

: 158137-46-3
2α,9α,10β-triacetyl taxicin-I

: 273926-82-2
C₃₆H₃₈O₁₀

Guidance literature:: Multi-step reaction with 11 steps

1.1: 81 percent / pyridine / 0.67 h / 20 °C

2.1: 81 percent / NaOMe / CH₂Cl₂; methanol / 24 h / 0 °C

3.1: 88 percent / pyridine / CH₂Cl₂ / 0.5 h / 0 °C

4.1: 100 percent / TBAF / tetrahydrofuran / 1 h / 20 °C

5.1: 83 percent / OsO₄; N-methylmorpholine N-oxide / tetrahydrofuran; H₂O; 2-methyl-propan-2-ol / 20 h / 20 °C

6.1: 95 percent / imidazole / dimethylformamide / 3 h / 20 °C

7.1: 83 percent / pyridine / 20 h / 20 °C

8.1: TBAF / tetrahydrofuran / 1 h / 20 °C

8.2: 76 percent / TBAOAc / butan-2-one / 20 h / Heating

9.1: 93 percent / DMAP / CH₂Cl₂ / 5 h / 20 °C

10.1: 64 percent / tetrahydrofuran; cyclohexane; diethyl ether / 0.33 h / -78 °C

11.1: 70 percent / n-methylmorpholine N-oxide; tetrapropylammonium perruthenate / CH₂Cl₂ / 3 h / 20 °C

With pyridine; 1H-imidazole; dmap; osmium(VIII) oxide; tetrapropylammonium perruthennate; tetrabutyl ammonium fluoride; sodium methylate; 4-methylmorpholine N-oxide; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; cyclohexane; water; N,N-dimethyl-formamide; tert-butyl alcohol; 1.1: silylation / 2.1: Deacetylation / 3.1: Carbonylation / 4.1: desilylation / 5.1: Oxidation / 6.1: silylation / 7.1: mesylation / 8.1: desylilation / 8.2: Cyclization / 9.1: Acetylation / 10.1: Phenylation / 11.1: Oxidation;
DOI:10.1016/S0040-4020(00)00073-9