Carbonic acid 5-(2-benzyloxycarbonylamino-ethyl)-2-ethoxycarbonyloxy-phenyl ester ethyl ester

Base Information

Chemical Name:Carbonic acid 5-(2-benzyloxycarbonylamino-ethyl)-2-ethoxycarbonyloxy-phenyl ester ethyl ester
CAS No.:37034-23-4
Molecular Formula:C₂₂H₂₅NO₈
Molecular Weight:431.442
Hs Code.:

Synonyms:Carbonic acid 5-(2-benzyloxycarbonylamino-ethyl)-2-ethoxycarbonyloxy-phenyl ester ethyl ester

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Chemical Property of Carbonic acid 5-(2-benzyloxycarbonylamino-ethyl)-2-ethoxycarbonyloxy-phenyl ester ethyl ester

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Technology Process of Carbonic acid 5-(2-benzyloxycarbonylamino-ethyl)-2-ethoxycarbonyloxy-phenyl ester ethyl ester

There total 4 articles about Carbonic acid 5-(2-benzyloxycarbonylamino-ethyl)-2-ethoxycarbonyloxy-phenyl ester ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 37034-22-3
N-benzyloxycarbonyl-3,4-dihydroxyphenylethylamine

: 541-41-3
chloroformic acid ethyl ester

: 37034-23-4
Carbonic acid 5-(2-benzyloxycarbonylamino-ethyl)-2-ethoxycarbonyloxy-phenyl ester ethyl ester

Guidance literature:: With dmap; In pyridine; at 80 ℃; for 4h;

Reference yield:

: 51-61-6
dopamine

: 37034-23-4
Carbonic acid 5-(2-benzyloxycarbonylamino-ethyl)-2-ethoxycarbonyloxy-phenyl ester ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 2 N NaOH / toluene; H₂O / 2 h / 5 - 10 °C

2: 58 percent / DMAP / pyridine / 4 h / 80 °C

With dmap; sodium hydroxide; In pyridine; water; toluene;

Reference yield:

: 501-53-1,94274-21-2
benzyl chloroformate

: 37034-23-4
Carbonic acid 5-(2-benzyloxycarbonylamino-ethyl)-2-ethoxycarbonyloxy-phenyl ester ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 2 N NaOH / toluene; H₂O / 2 h / 5 - 10 °C

2: 58 percent / DMAP / pyridine / 4 h / 80 °C

With dmap; sodium hydroxide; In pyridine; water; toluene;