(S)-N-((S)-((S)-2,2-dimethyl-1,3-dioxolan-4-yl)(p-methoxyphenyl)methyl)-2-methyl propane-2-sulfinamide

Base Information

Chemical Name:(S)-N-((S)-((S)-2,2-dimethyl-1,3-dioxolan-4-yl)(p-methoxyphenyl)methyl)-2-methyl propane-2-sulfinamide
CAS No.:1379528-94-5
Molecular Formula:C₁₇H₂₇NO₄S
Molecular Weight:341.472
Hs Code.:

Synonyms:(S)-N-((S)-((S)-2,2-dimethyl-1,3-dioxolan-4-yl)(p-methoxyphenyl)methyl)-2-methyl propane-2-sulfinamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-N-((S)-((S)-2,2-dimethyl-1,3-dioxolan-4-yl)(p-methoxyphenyl)methyl)-2-methyl propane-2-sulfinamide

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Technology Process of (S)-N-((S)-((S)-2,2-dimethyl-1,3-dioxolan-4-yl)(p-methoxyphenyl)methyl)-2-methyl propane-2-sulfinamide

There total 1 articles about (S)-N-((S)-((S)-2,2-dimethyl-1,3-dioxolan-4-yl)(p-methoxyphenyl)methyl)-2-methyl propane-2-sulfinamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 1262535-90-9
(S_S,E)-N-[(2S)-2,3-(isopropylidenedioxy)propylidene]-2-methyl-2-propanesulfinamide

: 13139-86-1
4-methoxyphenyl magnesium bromide

: 1379528-94-5
(S)-N-((S)-((S)-2,2-dimethyl-1,3-dioxolan-4-yl)(p-methoxyphenyl)methyl)-2-methyl propane-2-sulfinamide

Guidance literature:: In diethyl ether; at -78 ℃; for 5h; stereoselective reaction; Inert atmosphere;
DOI:10.1080/00397911.2011.563450

Reference yield: 80.0%

: 1379528-94-5
(S)-N-((S)-((S)-2,2-dimethyl-1,3-dioxolan-4-yl)(p-methoxyphenyl)methyl)-2-methyl propane-2-sulfinamide

: 1379528-98-9
(2S,3S)-3-amino-3-(4-methoxyphenyl)propane-1,2-diol hydrochloride

Guidance literature:: With hydrogenchloride; In methanol; at 20 ℃; for 12h; stereoselective reaction;
DOI:10.1080/00397911.2011.563450

Reference yield:

: 1379528-94-5
(S)-N-((S)-((S)-2,2-dimethyl-1,3-dioxolan-4-yl)(p-methoxyphenyl)methyl)-2-methyl propane-2-sulfinamide

: 220736-25-4,259794-13-3
(+)-(4S,5S)-5-(hydroxymethyl)-4-(4-methoxyphenyl)-1,3-oxazolidin-2-one

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogenchloride / methanol / 12 h / 20 °C

2: triethylamine / dichloromethane / 12 h / 0 °C / Inert atmosphere

3: sodium hydride / tetrahydrofuran; mineral oil / 2 h / 20 °C / Inert atmosphere

With hydrogenchloride; sodium hydride; triethylamine; In tetrahydrofuran; methanol; dichloromethane; mineral oil;
DOI:10.1080/00397911.2011.563450