trichloroethyl 6β-phenoxyacetamidopenicillanate-1β-sulfoxide

Base Information

• Chemical Name: trichloroethyl 6β-phenoxyacetamidopenicillanate-1β-sulfoxide
• CAS No.: 19474-21-6
• Molecular Formula: C₁₈H₁₉Cl₃N₂O₆S
• Molecular Weight: 497.784

Synonyms:trichloroethyl 6β-phenoxyacetamidopenicillanate-1β-sulfoxide

Chemical Property of trichloroethyl 6β-phenoxyacetamidopenicillanate-1β-sulfoxide

Chemical Property:

Purity/Quality:

98% ^*data from raw suppliers

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Technology Process of trichloroethyl 6β-phenoxyacetamidopenicillanate-1β-sulfoxide

There total 3 articles about trichloroethyl 6β-phenoxyacetamidopenicillanate-1β-sulfoxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

6β-(2-phenoxy-acetylamino)-penicillanic acid 2,2,2-trichloro-ethyl ester (19474-19-2) → trichloroethyl 6β-phenoxyacetamidopenicillanate-1β-sulfoxide (19474-21-6)

Guidance literature:

With dihydrogen peroxide; acetic acid; In dichloromethane; for 48h; Ambient temperature;

Reference yield:

phenoxymethylpenicillin sulfoxide (4888-90-8) + ethyl 2-(2,2,2-trichloroethyl)oxycarbonyloxyimino-2-cyanoacetate → trichloroethyl 6β-phenoxyacetamidopenicillanate-1β-sulfoxide (19474-21-6)

Guidance literature:

With sodium chloride; sodium hydrogencarbonate; triethylamine; citric acid; In water; ethyl acetate;

Reference yield:

1β-oxo-6β-(2-phenoxy-acetylamino)-1λ4-penicillanic acid 2,2,2-trichloro-ethyl ester (30199-55-4) → 1β-oxo-6α-(2-phenoxy-acetylamino)-1λ4-penicillanic acid 2,2,2-trichloro-ethyl ester (19474-21-6,27250-42-6,30199-55-4,90026-86-1)

Guidance literature:

DOI:10.1016/S0040-4039(01)98081-5

upstream raw materials:

6β-(2-phenoxy-acetylamino)-penicillanic acid 2,2,2-trichloro-ethyl ester

phenoxymethylpenicillin sulfoxide

1β-oxo-6β-(2-phenoxy-acetylamino)-1λ⁴-penicillanic acid 2,2,2-trichloro-ethyl ester

Downstream raw materials:

(R)-3-methyl-2-((1S)-7-oxo-3-phenoxymethyl-(1rH,5cH)-4-thia-2,6-diaza-bicyclo[3.2.0]hept-2-en-6-yl)-but-3-enoic acid 2,2,2-trichloro-ethyl ester

10-acetoxy-6β-(2-phenoxy-acetylamino)-penicillanic acid 2,2,2-trichloro-ethyl ester

3-Methyl-2-[3-oxo-4-(2-phenoxy-acetylamino)-3H-isothiazol-2-yl]-but-2-enoic acid 2,2,2-trichloro-ethyl ester

3-Methyl-2-[(2-phenoxymethyl-thiazole-4-carbonyl)-amino]-but-3-enoic acid 2,2,2-trichloro-ethyl ester

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