2,6-bis(3-pyridyl)phenyl benzyl ether

Base Information

Chemical Name:2,6-bis(3-pyridyl)phenyl benzyl ether
CAS No.:1176188-71-8
Molecular Formula:C₂₃H₁₈N₂O
Molecular Weight:338.409
Hs Code.:

Synonyms:2,6-bis(3-pyridyl)phenyl benzyl ether

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Chemical Property of 2,6-bis(3-pyridyl)phenyl benzyl ether

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Technology Process of 2,6-bis(3-pyridyl)phenyl benzyl ether

There total 3 articles about 2,6-bis(3-pyridyl)phenyl benzyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 1692-25-7
3-pyridylboronic acid

: 122110-76-3
2-(Benzyloxy)-1,3-dibromobenzene

: 1176188-79-6
2-(3-pyridyl)phenyl benzyl ether

: 1176188-71-8
2,6-bis(3-pyridyl)phenyl benzyl ether

Guidance literature:: With potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In water; N,N-dimethyl-formamide; at 85 ℃; for 48h;

Reference yield:

: 608-33-3
2,6-dibromophenol

: 100-39-0
benzyl bromide

: 1176188-71-8
2,6-bis(3-pyridyl)phenyl benzyl ether

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydride / mineral oil / 80 °C

2: potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / N,N-dimethyl-formamide

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium hydride; potassium carbonate; In N,N-dimethyl-formamide; mineral oil; 2: |Suzuki Coupling;
DOI:10.1021/cm5011604