Technology Process of C21H17N3O2S
There total 8 articles about C21H17N3O2S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
trifluoroacetic acid;
In
dichloromethane;
at 20 ℃;
for 2h;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: sulfuric acid / 2 h / Reflux
2: tris-(dibenzylideneacetone)dipalladium(0); calcium acetate; tricyclohexylphosphine / 1,4-dioxane / 12 h / 90 °C / Inert atmosphere
3: tetrakis(triphenylphosphine) palladium(0); sodium carbonate / water; 1,4-dioxane / 18 h / 90 °C / Inert atmosphere
4: trifluoroacetic acid / dichloromethane / 2 h / 20 °C
With
tris-(dibenzylideneacetone)dipalladium(0); tetrakis(triphenylphosphine) palladium(0); sulfuric acid; calcium acetate; sodium carbonate; trifluoroacetic acid; tricyclohexylphosphine;
In
1,4-dioxane; dichloromethane; water;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: tris-(dibenzylideneacetone)dipalladium(0); calcium acetate; tricyclohexylphosphine / 1,4-dioxane / 12 h / 90 °C / Inert atmosphere
2: tetrakis(triphenylphosphine) palladium(0); sodium carbonate / water; 1,4-dioxane / 18 h / 90 °C / Inert atmosphere
3: trifluoroacetic acid / dichloromethane / 2 h / 20 °C
With
tris-(dibenzylideneacetone)dipalladium(0); tetrakis(triphenylphosphine) palladium(0); calcium acetate; sodium carbonate; trifluoroacetic acid; tricyclohexylphosphine;
In
1,4-dioxane; dichloromethane; water;