(E)-N-(1-(4-methoxyphenyl)-4-methylpent-1-yn-3-ylidene)-2-methylpropan-2-amine N-oxide

Base Information

Chemical Name:(E)-N-(1-(4-methoxyphenyl)-4-methylpent-1-yn-3-ylidene)-2-methylpropan-2-amine N-oxide
CAS No.:1291087-50-7
Molecular Formula:C₁₇H₂₃NO₂
Molecular Weight:273.375
Hs Code.:

Synonyms:(E)-N-(1-(4-methoxyphenyl)-4-methylpent-1-yn-3-ylidene)-2-methylpropan-2-amine N-oxide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-N-(1-(4-methoxyphenyl)-4-methylpent-1-yn-3-ylidene)-2-methylpropan-2-amine N-oxide

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Technology Process of (E)-N-(1-(4-methoxyphenyl)-4-methylpent-1-yn-3-ylidene)-2-methylpropan-2-amine N-oxide

There total 1 articles about (E)-N-(1-(4-methoxyphenyl)-4-methylpent-1-yn-3-ylidene)-2-methylpropan-2-amine N-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 85664-55-7
(Z)-2-methyl-N-(2-methylpropylidene)propan-2-amine N-oxide

: 768-60-5
4-methoxyphenylacetylen

: 1291087-50-7
(E)-N-(1-(4-methoxyphenyl)-4-methylpent-1-yn-3-ylidene)-2-methylpropan-2-amine N-oxide

Guidance literature:: 4-methoxyphenylacetylen; With zinc(II) triflate; triethylamine; In α,α,α-trifluorotoluene; at 20 ℃; for 0.333333h;

(Z)-2-methyl-N-(2-methylpropylidene)propan-2-amine N-oxide; With 3,5,3',5'-tetra-tert-butyl-4,4'-diphenoquinone; oxygen; In α,α,α-trifluorotoluene; at 60 ℃; for 24h;
DOI:10.1021/ol200849k

Reference yield: 88.0%

: 1291087-50-7
(E)-N-(1-(4-methoxyphenyl)-4-methylpent-1-yn-3-ylidene)-2-methylpropan-2-amine N-oxide

: 1346238-51-4
1-(4-methoxyphenyl)-4-methylpent-1-yn-3-one oxime

Guidance literature:: With titanium tetrachloride; In dichloromethane; at 50 ℃; for 24h; Inert atmosphere;
DOI:10.1002/adsc.201100327

Reference yield:

: 1291087-50-7
(E)-N-(1-(4-methoxyphenyl)-4-methylpent-1-yn-3-ylidene)-2-methylpropan-2-amine N-oxide

: 1346238-46-7
3-isopropyl-5-(4-methoxyphenyl)isoxazole

Guidance literature:: Multi-step reaction with 2 steps

1: titanium tetrachloride / dichloromethane / 24 h / 50 °C / Inert atmosphere

2: gold(III) chloride / dichloromethane / 20 h / 50 °C / Inert atmosphere

With gold(III) chloride; titanium tetrachloride; In dichloromethane;
DOI:10.1002/adsc.201100327