10-phenyldispiro(acridine-9(10H),3'-[1,2]dioxetane-4',2''-tricyclo[3.3.1.1^3,7]decane)

Base Information

• Chemical Name: 10-phenyldispiro(acridine-9(10H),3'-[1,2]dioxetane-4',2''-tricyclo[3.3.1.1^3,7]decane)
• CAS No.: 206645-82-1
• Molecular Formula: C₂₉H₂₇NO₂
• Molecular Weight: 421.539

Synonyms:10-phenyldispiro(acridine-9(10H),3'-[1,2]dioxetane-4',2''-tricyclo[3.3.1.1^3,7]decane)

Chemical Property of 10-phenyldispiro(acridine-9(10H),3'-[1,2]dioxetane-4',2''-tricyclo[3.3.1.1^3,7]decane)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 10-phenyldispiro(acridine-9(10H),3'-[1,2]dioxetane-4',2''-tricyclo[3.3.1.1^3,7]decane)

There total 3 articles about 10-phenyldispiro(acridine-9(10H),3'-[1,2]dioxetane-4',2''-tricyclo[3.3.1.1^3,7]decane) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

9,10-dihydro-10-phenyl-9-(tricyclo[3.3.1.13,7]decylidene)acridine (192184-77-3) → 10-phenyldispiro(acridine-9(10H),3'-[1,2]dioxetane-4',2''-tricyclo[3.3.1.13,7]decane) (206645-82-1)

Guidance literature:

With polymer supported Rose-Bengal; oxygen; In dichloromethane; at -78 ℃; for 2h; Yield given; Irradiation;

DOI:10.3987/COM-97-S(N)85

Reference yield:

2-Adamantanone (700-58-3) → 10-phenyldispiro(acridine-9(10H),3'-[1,2]dioxetane-4',2''-tricyclo[3.3.1.13,7]decane) (206645-82-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 51 percent / LiAlH₄, TiCl₃, Et₃N / tetrahydrofuran / 17 h / Heating

2: polymer supported Rose-Bengal, O₂ / CH₂Cl₂ / 2 h / -78 °C / Irradiation

With lithium aluminium tetrahydride; titanium(III) chloride; polymer supported Rose-Bengal; oxygen; triethylamine; In tetrahydrofuran; dichloromethane;

DOI:10.3987/COM-97-S(N)85

Reference yield:

9,10-dihydro-10-methyl-9-(tricyclo[3.3.1.13,7]decylidene)acridine (86042-97-9) → 10-phenyldispiro(acridine-9(10H),3'-[1,2]dioxetane-4',2''-tricyclo[3.3.1.13,7]decane) (206645-82-1)

Guidance literature:

Multi-step reaction with 3 steps

1: o-xylene / 25 °C / Ea; ΔH(excit.); -ΔS(excit.)

2: 51 percent / LiAlH₄, TiCl₃, Et₃N / tetrahydrofuran / 17 h / Heating

3: polymer supported Rose-Bengal, O₂ / CH₂Cl₂ / 2 h / -78 °C / Irradiation

With lithium aluminium tetrahydride; titanium(III) chloride; polymer supported Rose-Bengal; oxygen; triethylamine; In tetrahydrofuran; dichloromethane; o-xylene;

DOI:10.3987/COM-97-S(N)85

upstream raw materials:

9,10-dihydro-10-phenyl-9-(tricyclo[3.3.1.1^3,7]decylidene)acridine

2-Adamantanone

9,10-dihydro-10-methyl-9-(tricyclo[3.3.1.1^3,7]decylidene)acridine

Downstream raw materials:

2-Adamantanone

10-phenylacridin-9(10H)-one

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 206645-82-1 10-phenyldispiro(acridine-9(10H),3'-[1,2]dioxetane-4',2''-tricyclo[3.3.1.1^3,7]decane)

Send

Send

Metric Ton KG G Pound L ML

Send

Send