5,6,7,8-tetrahydro-7-phenyldibenzoxanthylium tetrafluoroborate

Base Information

Chemical Name:5,6,7,8-tetrahydro-7-phenyldibenzoxanthylium tetrafluoroborate
CAS No.:53217-56-4
Molecular Formula:BF₄*C₂₇H₂₁O
Molecular Weight:448.268
Hs Code.:

5,6,7,8-tetrahydro-7-phenyldibenzo<c,h>xanthylium tetrafluoroborate

Synonyms:5,6,7,8-tetrahydro-7-phenyldibenzoxanthylium tetrafluoroborate

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Chemical Property of 5,6,7,8-tetrahydro-7-phenyldibenzoxanthylium tetrafluoroborate

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Technology Process of 5,6,7,8-tetrahydro-7-phenyldibenzoxanthylium tetrafluoroborate

There total 4 articles about 5,6,7,8-tetrahydro-7-phenyldibenzoxanthylium tetrafluoroborate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 6261-32-1
2-benzylidene-1-tetralone

: 529-34-0
3,4-dihydronaphthalene-1(2H)-one

: 53217-56-4
5,6,7,8-tetrahydro-7-phenyldibenzoxanthylium tetrafluoroborate

Guidance literature:: With boron trifluoride diethyl etherate; at 120 - 130 ℃; for 4h;

Reference yield: 70.0%

: 5706-12-7
(E)-2-benzylidene-2,3-dihydro-1H-inden-1-one

: 529-34-0
3,4-dihydronaphthalene-1(2H)-one

: 53217-56-4
5,6,7,8-tetrahydro-7-phenyldibenzoxanthylium tetrafluoroborate

Guidance literature:: With boron trifluoride diethyl etherate; at 120 - 130 ℃; for 4h;

Reference yield:

: 100-52-7
benzaldehyde

: 53217-56-4
5,6,7,8-tetrahydro-7-phenyldibenzoxanthylium tetrafluoroborate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydroxide / methanol; water / 0 - 20 °C / Inert atmosphere; Schlenk technique

2: tetrahydrofuran / 12 h / 0 - 85 °C / Schlenk technique; Inert atmosphere

With sodium hydroxide; In tetrahydrofuran; methanol; water;
DOI:10.1002/chem.202000412