(+/-)-trans-2-<<<(2-phenylcyclopropyl)amino>carbonyl>oxy>ethyl-3-pyridine carboxylate

Base Information

Chemical Name:(+/-)-trans-2-<<<(2-phenylcyclopropyl)amino>carbonyl>oxy>ethyl-3-pyridine carboxylate
CAS No.:133941-16-9
Molecular Formula:C₁₈H₁₈N₂O₄
Molecular Weight:326.352
Hs Code.:

Synonyms:(+/-)-trans-2-<<<(2-phenylcyclopropyl)amino>carbonyl>oxy>ethyl-3-pyridine carboxylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (+/-)-trans-2-<<<(2-phenylcyclopropyl)amino>carbonyl>oxy>ethyl-3-pyridine carboxylate

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Technology Process of (+/-)-trans-2-<<<(2-phenylcyclopropyl)amino>carbonyl>oxy>ethyl-3-pyridine carboxylate

There total 2 articles about (+/-)-trans-2-<<<(2-phenylcyclopropyl)amino>carbonyl>oxy>ethyl-3-pyridine carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 59-67-6
nicotinic acid

: 133941-14-7
2-bromoethyl (+/-)-trans-(2-phenylcyclopropyl)carbomate

: 133941-16-9
(+/-)-trans-2-<<<(2-phenylcyclopropyl)amino>carbonyl>oxy>ethyl-3-pyridine carboxylate

Guidance literature:: With triethylamine; In N,N-dimethyl-formamide; for 48h; Ambient temperature;
DOI:10.1002/jps.2600800313

Reference yield:

: 1986-47-6,2208-35-7,2337-86-2,4548-34-9,37388-05-9,54779-58-7,61-81-4
tranylcypromine hydrochloride

: 133941-16-9
(+/-)-trans-2-<<<(2-phenylcyclopropyl)amino>carbonyl>oxy>ethyl-3-pyridine carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 65 percent / Et₃N / CHCl₃ / 24 h

2: 65 percent / Et₃N / dimethylformamide / 48 h / Ambient temperature

With triethylamine; In chloroform; N,N-dimethyl-formamide;
DOI:10.1002/jps.2600800313