C₁₆H₁₇BrO₅S

Base Information

Chemical Name:C₁₆H₁₇BrO₅S
CAS No.:1394902-91-0
Molecular Formula:C₁₆H₁₇BrO₅S
Molecular Weight:401.278
Hs Code.:

C<sub>16</sub>H<sub>17</sub>BrO<sub>5</sub>S

Synonyms:C₁₆H₁₇BrO₅S

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Chemical Property of C₁₆H₁₇BrO₅S

Chemical Property:

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Technology Process of C₁₆H₁₇BrO₅S

There total 1 articles about C₁₆H₁₇BrO₅S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6626-15-9
4-Bromoresorcinol

: 98-59-9
p-toluenesulfonyl chloride

: 3188-13-4
ethyl chloromethyl ether

: 1394902-91-0
C₁₆H₁₇BrO₅S

Guidance literature:: 4-Bromoresorcinol; p-toluenesulfonyl chloride; With potassium carbonate; In acetone; for 12h; Inert atmosphere; Reflux;

ethyl chloromethyl ether; In acetone; for 6h; Inert atmosphere; Reflux;
DOI:10.1021/ol302132s

Reference yield:

: 1394902-91-0
C₁₆H₁₇BrO₅S

: C₉H₁₁BrO₃

Guidance literature:: With potassium hydroxide; In ethanol; water; at 100 ℃; for 2h; Inert atmosphere;
DOI:10.1021/ol302132s

Reference yield:

: 1394902-91-0
C₁₆H₁₇BrO₅S

: 1394902-93-2
C₁₆H₂₅BO₅

Guidance literature:: Multi-step reaction with 5 steps

1.1: potassium hydroxide / ethanol; water / 2 h / 100 °C / Inert atmosphere

2.1: potassium carbonate / acetone / 3 h / Inert atmosphere; Reflux

3.1: n-butyllithium / hexane; tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere

3.2: 2 h / -78 - 20 °C

4.1: potassium dihydrogenphosphate / water; diethyl ether / Inert atmosphere

5.1: magnesium sulfate / dichloromethane; water / 12 h / 20 °C / Inert atmosphere

With potassium dihydrogenphosphate; n-butyllithium; magnesium sulfate; potassium carbonate; potassium hydroxide; In tetrahydrofuran; diethyl ether; ethanol; hexane; dichloromethane; water; acetone;
DOI:10.1021/ol302132s