Hydroiodid v. 1-Phenyl-2-methylthio-Δ²-imidazolin

Base Information

• Chemical Name: Hydroiodid v. 1-Phenyl-2-methylthio-Δ²-imidazolin
• CAS No.: 61406-15-3
• Molecular Formula: C₁₀H₁₂N₂S*HI
• Molecular Weight: 320.197

Synonyms:Hydroiodid v. 1-Phenyl-2-methylthio-Δ²-imidazolin

Chemical Property of Hydroiodid v. 1-Phenyl-2-methylthio-Δ²-imidazolin

Chemical Property:

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Technology Process of Hydroiodid v. 1-Phenyl-2-methylthio-Δ²-imidazolin

There total 1 articles about Hydroiodid v. 1-Phenyl-2-methylthio-Δ²-imidazolin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C9H10N2S + methyl iodide (74-88-4) → Hydroiodid v. 1-Phenyl-2-methylthio-Δ2-imidazolin (61406-15-3)

Guidance literature:

In methanol;

DOI:10.1016/j.bioorg.2019.103480

Reference yield: 71.0%

Hydroiodid v. 1-Phenyl-2-methylthio-Δ2-imidazolin (61406-15-3) → 1-phenyl-2-hydrazinoimidazoline hydroiodide

Guidance literature:

With hydrazine hydrate; In methanol; for 30h; Heating;

DOI:10.1016/j.ejmech.2006.06.013

Reference yield:

Hydroiodid v. 1-Phenyl-2-methylthio-Δ2-imidazolin (61406-15-3) → methyl 2-(4-oxo-8-phenyl-2H-3,4,6,7-tetrahydroimidazo[2,1-c][1,2,4]triazin-3-yl)acetate

Guidance literature:

Multi-step reaction with 2 steps

1: 71 percent / hydrazine hydrate / methanol / 30 h / Heating

2: 57 percent / Et₃N / butan-1-ol / 6 h / Heating

With hydrazine hydrate; triethylamine; In methanol; butan-1-ol;

DOI:10.1016/j.ejmech.2006.06.013

upstream raw materials:

methyl iodide

Downstream raw materials:

3-(2-furanyl)-8-phenyl-7,8-dihydroimidazo[2,1-c][1,2,4]triazin-4(6H)-one

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