3-(benzothiazol-2-yl)-1-(3,4,6-tri-O-benzyl-β-D-glucopyranosyl)-1H-indole

Base Information

Chemical Name:3-(benzothiazol-2-yl)-1-(3,4,6-tri-O-benzyl-β-D-glucopyranosyl)-1H-indole
CAS No.:869585-14-8
Molecular Formula:C₄₂H₃₈N₂O₅S
Molecular Weight:682.84
Hs Code.:

Synonyms:3-(benzothiazol-2-yl)-1-(3,4,6-tri-O-benzyl-β-D-glucopyranosyl)-1H-indole

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Chemical Property of 3-(benzothiazol-2-yl)-1-(3,4,6-tri-O-benzyl-β-D-glucopyranosyl)-1H-indole

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Technology Process of 3-(benzothiazol-2-yl)-1-(3,4,6-tri-O-benzyl-β-D-glucopyranosyl)-1H-indole

There total 4 articles about 3-(benzothiazol-2-yl)-1-(3,4,6-tri-O-benzyl-β-D-glucopyranosyl)-1H-indole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 31224-76-7
2-(1H-indol-3-yl)benzo[d]thiazole

: 1011723-04-8
glucal epoxide

: 869585-14-8
3-(benzothiazol-2-yl)-1-(3,4,6-tri-O-benzyl-β-D-glucopyranosyl)-1H-indole

: 869585-20-6
3-(benzothiazol-2-yl)-1-(3,4,6-tri-O-benzyl-β-D-mannopyranosyl)-1H-indole

Guidance literature:: 2-(1H-indol-3-yl)benzo[d]thiazole; With 18-crown-6 ether; sodium hydride; In acetonitrile; at 40 ℃; for 0.5h;

glucal epoxide; In acetonitrile; at 60 ℃; for 3h;
DOI:10.1135/cccc20050487

Reference yield: 44.0%

: 31224-76-7
2-(1H-indol-3-yl)benzo[d]thiazole

: 118243-90-6
3,4,6-tri-O-benzyl-1,2-O-sulfinyl-α-D-glucopyranoside

: 869585-14-8
3-(benzothiazol-2-yl)-1-(3,4,6-tri-O-benzyl-β-D-glucopyranosyl)-1H-indole

Guidance literature:: 2-(1H-indol-3-yl)benzo[d]thiazole; With potassium hydroxide; sodium sulfate; In N,N-dimethyl-formamide; at 20 ℃; for 0.5h;

3,4,6-tri-O-benzyl-1,2-O-sulfinyl-α-D-glucopyranoside; In N,N-dimethyl-formamide; for 0.5h;
DOI:10.1135/cccc20050487

Reference yield:

: 487-89-8,1228547-52-1
Indole-3-carboxaldehyde

: 869585-14-8
3-(benzothiazol-2-yl)-1-(3,4,6-tri-O-benzyl-β-D-glucopyranosyl)-1H-indole

Guidance literature:: Multi-step reaction with 2 steps

1.1: 54 percent / aq. HCl / methanol / 0.5 h / Heating

2.1: NaH; 18-crown-6 / acetonitrile / 0.5 h / 40 °C

2.2: 75 percent / acetonitrile / 3 h / 60 °C

With hydrogenchloride; 18-crown-6 ether; sodium hydride; In methanol; acetonitrile;
DOI:10.1135/cccc20050487